Beilstein J. Org. Chem.2007,3, No. 11, doi:10.1186/1860-5397-3-11
. Analysis of the 1H NMR spectra of 4a-d provided answers on the chemoselectivity of the cyclocondensation. The δ values of the most carbon signals could be determined and assigned to the corresponding carbon atoms. For example, the 13C NMR spectrum of compound 4b revealed fourteen distinctive carbon signals
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Graphical Abstract
Scheme 1:
Synthesis of triazoloquinazolinones 4a-dvia microwave irradiation.