data_he015 _audit_creation_date 2020-06-11 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _shelx_SHELXL_version_number '2018/1' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic '[5,15-dibromo-10,20-di(pentan-3-yl)porphyrinato]nickel(II)' _chemical_formula_moiety 'C30 H30 Br2 N4 Ni' _chemical_formula_sum 'C30 H30 Br2 N4 Ni' _chemical_formula_weight 665.11 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Br' 'Br' -0.6763 1.2805 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Ni' 'Ni' -3.0029 0.5091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 15 _space_group_name_H-M_alt 'C 1 2/c 1' _space_group_name_Hall '-C 2yc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 44.0507(16) _cell_length_b 10.2192(4) _cell_length_c 11.8461(4) _cell_angle_alpha 90 _cell_angle_beta 91.771(3) _cell_angle_gamma 90 _cell_volume 5330.1(3) _cell_formula_units_Z 8 _cell_measurement_reflns_used 9909 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 67.00 _cell_measurement_theta_min 4.02 _shelx_estimated_absorpt_T_max 0.796 _shelx_estimated_absorpt_T_min 0.286 _exptl_absorpt_coefficient_mu 4.768 _exptl_absorpt_correction_T_max 0.7965 _exptl_absorpt_correction_T_min 0.2862 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'Program Sadabs' _exptl_absorpt_special_details ? _exptl_crystal_colour red _exptl_crystal_colour_primary red _exptl_crystal_density_diffrn 1.658 _exptl_crystal_density_meas . _exptl_crystal_density_method 'not measured' _exptl_crystal_description plate _exptl_crystal_F_000 2688 _exptl_crystal_size_max 0.35 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.05 _exptl_special_details ; ? ; _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0810 _diffrn_reflns_av_unetI/netI 0.0474 _diffrn_reflns_Laue_measured_fraction_full 0.971 _diffrn_reflns_Laue_measured_fraction_max 0.971 _diffrn_reflns_limit_h_max 52 _diffrn_reflns_limit_h_min -49 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 18037 _diffrn_reflns_point_group_measured_fraction_full 0.971 _diffrn_reflns_point_group_measured_fraction_max 0.971 _diffrn_reflns_theta_full 66.994 _diffrn_reflns_theta_max 66.994 _diffrn_reflns_theta_min 2.007 _diffrn_ambient_temperature 100.15 _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.971 _diffrn_measured_fraction_theta_max 0.971 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_source ? _diffrn_standards_number 0 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 4210 _reflns_number_total 4611 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 2008)' _refine_diff_density_max 1.169 _refine_diff_density_min -1.530 _refine_diff_density_rms 0.121 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.032 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 348 _refine_ls_number_reflns 4611 _refine_ls_number_restraints 18 _refine_ls_R_factor_all 0.0476 _refine_ls_R_factor_gt 0.0443 _refine_ls_restrained_S_all 1.030 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0736P)^2^+20.0009P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1181 _refine_ls_wR_factor_ref 0.1209 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All C(H,H,H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Uiso/Uaniso restraints and constraints C106 \\sim C105 \\sim C104: within 2A with sigma of 0.001 and sigma for terminal atoms of 0.002 3. Others Fixed Sof: H10F(0.5) H10G(0.5) H10H(0.5) H10I(0.5) C105(0.5) H10J(0.5) H10K(0.5) H10L(0.5) C106(0.5) H10M(0.5) H10N(0.5) H10O(0.5) 4.a Ternary CH refined with riding coordinates: C101(H101), C201(H201) 4.b Secondary CH2 refined with riding coordinates: C102(H10A,H10B), C104(H10F,H10G), C104(H10H,H10I), C202(H20A,H20B), C204(H20F, H20G) 4.c Aromatic/amide H refined with riding coordinates: C7(H7), C8(H8), C12(H12), C13(H13), C17(H17), C18(H18), C2(H2), C3(H3) 4.d Idealised Me refined as rotating group: C103(H10C,H10D,H10E), C105(H10J,H10K,H10L), C106(H10M,H10N,H10O), C203(H20C, H20D,H20E), C205(H20H,H20I,H20J) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary ? _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ni1 Ni 0.12370(2) 0.24209(5) 0.06298(4) 0.01115(16) Uani 1 1 d . . . . . N22 N 0.13072(6) 0.1142(3) 0.1784(2) 0.0136(6) Uani 1 1 d . . . . . N23 N 0.08302(6) 0.2599(3) 0.1113(2) 0.0140(6) Uani 1 1 d . . . . . N24 N 0.11607(6) 0.3611(3) -0.0593(2) 0.0138(6) Uani 1 1 d . . . . . N21 N 0.16473(6) 0.2259(3) 0.0157(2) 0.0124(5) Uani 1 1 d . . . . . C6 C 0.15314(8) 0.0200(3) 0.1807(3) 0.0157(7) Uani 1 1 d . . . . . C7 C 0.14974(8) -0.0661(4) 0.2741(3) 0.0220(8) Uani 1 1 d . . . . . H7 H 0.161696 -0.141161 0.291696 0.026 Uiso 1 1 calc R . . . . C8 C 0.12619(8) -0.0200(4) 0.3325(3) 0.0241(8) Uani 1 1 d . . . . . H8 H 0.119174 -0.054399 0.401443 0.029 Uiso 1 1 calc R . . . . C9 C 0.11366(8) 0.0895(3) 0.2725(3) 0.0174(7) Uani 1 1 d . . . . . C10 C 0.08668(8) 0.1535(3) 0.2980(3) 0.0167(7) Uani 1 1 d . . . . . C11 C 0.07163(8) 0.2271(3) 0.2157(3) 0.0156(7) Uani 1 1 d . . . . . C12 C 0.04027(8) 0.2638(3) 0.2188(3) 0.0200(7) Uani 1 1 d . . . . . H12 H 0.027581 0.256119 0.281863 0.024 Uiso 1 1 calc R . . . . C13 C 0.03199(8) 0.3111(3) 0.1161(3) 0.0208(7) Uani 1 1 d . . . . . H13 H 0.012237 0.339088 0.092406 0.025 Uiso 1 1 calc R . . . . C14 C 0.05868(8) 0.3114(3) 0.0494(3) 0.0168(7) Uani 1 1 d . . . . . C15 C 0.06102(8) 0.3620(3) -0.0572(3) 0.0177(7) Uani 1 1 d . . . . . C16 C 0.08796(8) 0.3907(3) -0.1087(3) 0.0167(7) Uani 1 1 d . . . . . C17 C 0.09162(8) 0.4692(4) -0.2064(3) 0.0196(7) Uani 1 1 d . . . . . H17 H 0.075888 0.497194 -0.257495 0.024 Uiso 1 1 calc R . . . . C18 C 0.12116(8) 0.4967(4) -0.2133(3) 0.0194(7) Uani 1 1 d . . . . . H18 H 0.130138 0.551143 -0.268044 0.023 Uiso 1 1 calc R . . . . C19 C 0.13697(8) 0.4282(3) -0.1223(3) 0.0152(7) Uani 1 1 d . . . . . C20 C 0.16812(8) 0.4184(3) -0.1088(3) 0.0146(7) Uani 1 1 d . . . . . C1 C 0.18073(7) 0.3135(3) -0.0491(3) 0.0134(6) Uani 1 1 d . . . . . C2 C 0.21103(8) 0.2637(3) -0.0631(3) 0.0165(7) Uani 1 1 d . . . . . H2 H 0.226934 0.306784 -0.100711 0.020 Uiso 1 1 calc R . . . . C3 C 0.21274(8) 0.1456(3) -0.0137(3) 0.0164(7) Uani 1 1 d . . . . . H3 H 0.229602 0.087675 -0.013409 0.020 Uiso 1 1 calc R . . . . C4 C 0.18422(8) 0.1237(3) 0.0388(3) 0.0144(7) Uani 1 1 d . . . . . C5 C 0.17771(7) 0.0216(3) 0.1104(3) 0.0150(7) Uani 1 1 d . . . . . Br2 Br 0.02437(2) 0.41101(5) -0.13408(4) 0.03465(16) Uani 1 1 d . . . . . Br1 Br 0.20646(2) -0.11568(4) 0.12592(3) 0.02254(14) Uani 1 1 d . . . . . C101 C 0.07141(9) 0.1307(4) 0.4111(3) 0.0260(8) Uani 1 1 d . . . . . H101 H 0.055618 0.200836 0.414133 0.031 Uiso 1 1 calc R . . . . C102 C 0.09126(12) 0.1536(5) 0.5155(4) 0.0443(12) Uani 1 1 d . . . . . H10A H 0.078860 0.139149 0.582665 0.053 Uiso 1 1 calc R . . . . H10B H 0.107625 0.087121 0.517356 0.053 Uiso 1 1 calc R . . . . C103 C 0.10530(15) 0.2838(6) 0.5249(4) 0.0595(15) Uani 1 1 d . . . . . H10C H 0.117928 0.288388 0.594393 0.089 Uiso 1 1 calc GR . . . . H10D H 0.089380 0.350673 0.527043 0.089 Uiso 1 1 calc GR . . . . H10E H 0.117955 0.299195 0.459625 0.089 Uiso 1 1 calc GR . . . . C104 C 0.05331(13) 0.0035(6) 0.4121(5) 0.0558(12) Uani 1 1 d . U . . . H10F H 0.046833 -0.017446 0.333397 0.067 Uiso 0.5 1 calc R . P A 1 H10G H 0.067049 -0.067493 0.438796 0.067 Uiso 0.5 1 calc R . P A 1 H10H H 0.068350 -0.066892 0.427123 0.067 Uiso 0.5 1 calc R . P B 2 H10I H 0.040656 0.008014 0.479619 0.067 Uiso 0.5 1 calc R . P B 2 C105 C 0.0264(3) 0.0023(11) 0.4815(10) 0.0573(14) Uani 0.5 1 d . U P C 1 H10J H 0.013444 0.077134 0.461308 0.086 Uiso 0.5 1 calc GR . P C 1 H10K H 0.032691 0.008034 0.561394 0.086 Uiso 0.5 1 calc GR . P C 1 H10L H 0.015106 -0.079114 0.468124 0.086 Uiso 0.5 1 calc GR . P C 1 C106 C 0.0343(3) -0.0423(11) 0.3252(10) 0.0566(14) Uani 0.5 1 d . U P C 2 H10M H 0.028372 -0.132682 0.341064 0.085 Uiso 0.5 1 calc GR . P C 2 H10N H 0.045019 -0.039292 0.253917 0.085 Uiso 0.5 1 calc GR . P C 2 H10O H 0.016128 0.012833 0.319133 0.085 Uiso 0.5 1 calc GR . P C 2 C201 C 0.18927(8) 0.5126(3) -0.1691(3) 0.0161(7) Uani 1 1 d . . . . . H201 H 0.210179 0.494879 -0.137561 0.019 Uiso 1 1 calc R . . . . C202 C 0.18225(8) 0.6562(3) -0.1401(3) 0.0206(7) Uani 1 1 d . . . . . H20A H 0.162917 0.682020 -0.178686 0.025 Uiso 1 1 calc R . . . . H20B H 0.179527 0.663787 -0.057680 0.025 Uiso 1 1 calc R . . . . C203 C 0.20727(9) 0.7499(4) -0.1747(3) 0.0243(8) Uani 1 1 d . . . . . H20C H 0.202033 0.839165 -0.152342 0.036 Uiso 1 1 calc GR . . . . H20D H 0.209336 0.746247 -0.256804 0.036 Uiso 1 1 calc GR . . . . H20E H 0.226521 0.724313 -0.137302 0.036 Uiso 1 1 calc GR . . . . C204 C 0.19043(8) 0.4859(4) -0.2987(3) 0.0197(7) Uani 1 1 d . . . . . H20F H 0.179034 0.404593 -0.316500 0.024 Uiso 1 1 calc R . . . . H20G H 0.180210 0.558627 -0.339869 0.024 Uiso 1 1 calc R . . . . C205 C 0.22251(8) 0.4721(4) -0.3400(3) 0.0251(8) Uani 1 1 d . . . . . H20H H 0.221808 0.455057 -0.421486 0.038 Uiso 1 1 calc GR . . . . H20I H 0.232668 0.399151 -0.300676 0.038 Uiso 1 1 calc GR . . . . H20J H 0.233780 0.553160 -0.324674 0.038 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ni1 0.0133(3) 0.0103(3) 0.0098(3) 0.0014(2) 0.0005(2) 0.0020(2) N22 0.0158(14) 0.0132(14) 0.0118(13) -0.0009(10) 0.0013(11) 0.0026(10) N23 0.0169(14) 0.0116(13) 0.0134(13) 0.0010(10) 0.0001(10) 0.0007(11) N24 0.0153(14) 0.0138(14) 0.0124(13) 0.0010(11) 0.0014(10) 0.0025(11) N21 0.0160(14) 0.0114(13) 0.0097(13) -0.0007(10) 0.0000(10) 0.0016(11) C6 0.0188(16) 0.0116(16) 0.0164(17) -0.0001(13) -0.0029(13) 0.0008(13) C7 0.0253(19) 0.0198(18) 0.0208(18) 0.0097(15) 0.0004(14) 0.0060(15) C8 0.0258(19) 0.026(2) 0.0202(18) 0.0118(15) 0.0028(14) 0.0034(15) C9 0.0194(18) 0.0196(17) 0.0132(16) 0.0028(13) 0.0002(13) -0.0009(14) C10 0.0201(17) 0.0154(17) 0.0147(16) -0.0002(13) 0.0033(13) -0.0024(13) C11 0.0172(17) 0.0121(16) 0.0178(16) -0.0015(13) 0.0041(13) -0.0030(13) C12 0.0183(17) 0.0167(17) 0.0255(19) 0.0027(14) 0.0071(14) 0.0011(13) C13 0.0160(17) 0.0184(18) 0.0281(19) 0.0048(15) 0.0044(14) 0.0051(13) C14 0.0155(16) 0.0117(16) 0.0232(17) -0.0004(13) 0.0019(13) 0.0024(13) C15 0.0158(16) 0.0147(17) 0.0223(18) 0.0039(14) -0.0045(13) 0.0034(13) C16 0.0177(17) 0.0164(17) 0.0160(16) -0.0013(13) -0.0012(13) 0.0031(13) C17 0.0196(17) 0.0241(19) 0.0150(16) 0.0054(14) -0.0025(13) 0.0067(14) C18 0.0230(18) 0.0194(18) 0.0158(17) 0.0062(14) -0.0004(13) 0.0039(14) C19 0.0203(17) 0.0134(16) 0.0120(15) 0.0004(13) 0.0015(13) 0.0005(13) C20 0.0206(17) 0.0158(16) 0.0075(14) -0.0012(12) 0.0024(12) -0.0007(13) C1 0.0161(16) 0.0148(16) 0.0093(14) -0.0013(12) -0.0003(12) -0.0009(13) C2 0.0145(16) 0.0211(18) 0.0140(16) -0.0024(13) 0.0019(12) 0.0004(13) C3 0.0154(16) 0.0209(17) 0.0129(15) -0.0010(13) 0.0015(12) 0.0057(14) C4 0.0156(16) 0.0153(17) 0.0123(15) -0.0037(12) -0.0012(12) 0.0023(13) C5 0.0176(16) 0.0141(16) 0.0132(16) -0.0026(13) -0.0022(12) 0.0045(13) Br2 0.0163(2) 0.0521(3) 0.0353(3) 0.0215(2) -0.00337(17) 0.00609(17) Br1 0.0260(2) 0.0186(2) 0.0231(2) 0.00424(14) 0.00248(15) 0.01147(14) C101 0.027(2) 0.032(2) 0.0197(18) 0.0048(16) 0.0087(15) 0.0036(16) C102 0.051(3) 0.059(3) 0.023(2) 0.000(2) 0.0052(19) 0.014(2) C103 0.080(4) 0.069(4) 0.029(3) -0.002(3) -0.004(2) -0.009(3) C104 0.057(3) 0.049(3) 0.063(3) 0.015(2) 0.016(2) -0.021(2) C105 0.059(3) 0.049(3) 0.065(3) 0.016(3) 0.015(3) -0.020(2) C106 0.058(3) 0.048(3) 0.064(3) 0.017(3) 0.014(2) -0.022(2) C201 0.0170(16) 0.0147(17) 0.0166(17) 0.0014(13) 0.0012(13) -0.0009(13) C202 0.0251(18) 0.0163(18) 0.0205(17) 0.0021(14) 0.0015(14) -0.0012(14) C203 0.031(2) 0.0167(18) 0.0257(19) 0.0043(14) 0.0025(15) -0.0038(15) C204 0.0259(19) 0.0199(18) 0.0134(17) 0.0021(14) 0.0038(13) -0.0009(14) C205 0.027(2) 0.029(2) 0.0199(18) 0.0005(15) 0.0053(15) -0.0034(16) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ni1 N22 1.910(3) . ? Ni1 N23 1.907(3) . ? Ni1 N24 1.913(3) . ? Ni1 N21 1.916(3) . ? N22 C6 1.379(4) . ? N22 C9 1.386(4) . ? N23 C11 1.389(4) . ? N23 C14 1.384(4) . ? N24 C16 1.386(4) . ? N24 C19 1.384(4) . ? N21 C1 1.386(4) . ? N21 C4 1.374(4) . ? C6 C7 1.424(5) . ? C6 C5 1.386(5) . ? C7 H7 0.9500 . ? C7 C8 1.350(5) . ? C8 H8 0.9500 . ? C8 C9 1.427(5) . ? C9 C10 1.398(5) . ? C10 C11 1.384(5) . ? C10 C101 1.536(5) . ? C11 C12 1.433(5) . ? C12 H12 0.9500 . ? C12 C13 1.349(5) . ? C13 H13 0.9500 . ? C13 C14 1.437(5) . ? C14 C15 1.371(5) . ? C15 C16 1.383(5) . ? C15 Br2 1.896(3) . ? C16 C17 1.422(5) . ? C17 H17 0.9500 . ? C17 C18 1.336(5) . ? C18 H18 0.9500 . ? C18 C19 1.446(5) . ? C19 C20 1.380(5) . ? C20 C1 1.391(5) . ? C20 C201 1.532(5) . ? C1 C2 1.443(5) . ? C2 H2 0.9500 . ? C2 C3 1.342(5) . ? C3 H3 0.9500 . ? C3 C4 1.437(5) . ? C4 C5 1.380(5) . ? C5 Br1 1.895(3) . ? C101 H101 1.0000 . ? C101 C102 1.510(6) . ? C101 C104 1.526(6) . ? C102 H10A 0.9900 . ? C102 H10B 0.9900 . ? C102 C103 1.471(8) . ? C103 H10C 0.9800 . ? C103 H10D 0.9800 . ? C103 H10E 0.9800 . ? C104 H10F 0.9900 . ? C104 H10G 0.9900 . ? C104 H10H 0.9900 . ? C104 H10I 0.9900 . ? C104 C105 1.462(11) . ? C104 C106 1.388(13) . ? C105 H10J 0.9800 . ? C105 H10K 0.9800 . ? C105 H10L 0.9800 . ? C106 H10M 0.9800 . ? C106 H10N 0.9800 . ? C106 H10O 0.9800 . ? C201 H201 1.0000 . ? C201 C202 1.540(5) . ? C201 C204 1.561(5) . ? C202 H20A 0.9900 . ? C202 H20B 0.9900 . ? C202 C203 1.526(5) . ? C203 H20C 0.9800 . ? C203 H20D 0.9800 . ? C203 H20E 0.9800 . ? C204 H20F 0.9900 . ? C204 H20G 0.9900 . ? C204 C205 1.516(5) . ? C205 H20H 0.9800 . ? C205 H20I 0.9800 . ? C205 H20J 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N22 Ni1 N24 176.31(12) . . ? N22 Ni1 N21 90.97(12) . . ? N23 Ni1 N22 89.03(12) . . ? N23 Ni1 N24 91.25(12) . . ? N23 Ni1 N21 179.30(12) . . ? N24 Ni1 N21 88.80(11) . . ? C6 N22 Ni1 126.3(2) . . ? C6 N22 C9 105.2(3) . . ? C9 N22 Ni1 128.4(2) . . ? C11 N23 Ni1 127.8(2) . . ? C14 N23 Ni1 126.6(2) . . ? C14 N23 C11 105.6(3) . . ? C16 N24 Ni1 126.3(2) . . ? C19 N24 Ni1 128.2(2) . . ? C19 N24 C16 105.4(3) . . ? C1 N21 Ni1 127.3(2) . . ? C4 N21 Ni1 126.6(2) . . ? C4 N21 C1 106.0(3) . . ? N22 C6 C7 110.8(3) . . ? N22 C6 C5 123.5(3) . . ? C5 C6 C7 125.2(3) . . ? C6 C7 H7 126.8 . . ? C8 C7 C6 106.4(3) . . ? C8 C7 H7 126.8 . . ? C7 C8 H8 126.0 . . ? C7 C8 C9 108.1(3) . . ? C9 C8 H8 126.0 . . ? N22 C9 C8 109.4(3) . . ? N22 C9 C10 125.0(3) . . ? C10 C9 C8 125.3(3) . . ? C9 C10 C101 121.0(3) . . ? C11 C10 C9 119.6(3) . . ? C11 C10 C101 119.0(3) . . ? N23 C11 C12 109.5(3) . . ? C10 C11 N23 125.4(3) . . ? C10 C11 C12 124.4(3) . . ? C11 C12 H12 126.1 . . ? C13 C12 C11 107.7(3) . . ? C13 C12 H12 126.1 . . ? C12 C13 H13 126.5 . . ? C12 C13 C14 107.1(3) . . ? C14 C13 H13 126.5 . . ? N23 C14 C13 110.0(3) . . ? C15 C14 N23 123.5(3) . . ? C15 C14 C13 126.4(3) . . ? C14 C15 C16 125.2(3) . . ? C14 C15 Br2 117.1(3) . . ? C16 C15 Br2 117.5(3) . . ? N24 C16 C17 110.1(3) . . ? C15 C16 N24 122.4(3) . . ? C15 C16 C17 126.8(3) . . ? C16 C17 H17 126.2 . . ? C18 C17 C16 107.7(3) . . ? C18 C17 H17 126.2 . . ? C17 C18 H18 126.3 . . ? C17 C18 C19 107.5(3) . . ? C19 C18 H18 126.3 . . ? N24 C19 C18 109.2(3) . . ? C20 C19 N24 125.3(3) . . ? C20 C19 C18 125.1(3) . . ? C19 C20 C1 119.6(3) . . ? C19 C20 C201 121.2(3) . . ? C1 C20 C201 118.9(3) . . ? N21 C1 C20 125.3(3) . . ? N21 C1 C2 108.9(3) . . ? C20 C1 C2 124.7(3) . . ? C1 C2 H2 126.1 . . ? C3 C2 C1 107.8(3) . . ? C3 C2 H2 126.1 . . ? C2 C3 H3 126.5 . . ? C2 C3 C4 106.9(3) . . ? C4 C3 H3 126.5 . . ? N21 C4 C3 110.1(3) . . ? N21 C4 C5 123.8(3) . . ? C5 C4 C3 125.8(3) . . ? C6 C5 Br1 117.7(2) . . ? C4 C5 C6 124.0(3) . . ? C4 C5 Br1 117.9(3) . . ? C10 C101 H101 104.2 . . ? C102 C101 C10 115.7(3) . . ? C102 C101 H101 104.2 . . ? C102 C101 C104 114.5(4) . . ? C104 C101 C10 112.3(4) . . ? C104 C101 H101 104.2 . . ? C101 C102 H10A 108.4 . . ? C101 C102 H10B 108.4 . . ? H10A C102 H10B 107.4 . . ? C103 C102 C101 115.7(4) . . ? C103 C102 H10A 108.4 . . ? C103 C102 H10B 108.4 . . ? C102 C103 H10C 109.5 . . ? C102 C103 H10D 109.5 . . ? C102 C103 H10E 109.5 . . ? H10C C103 H10D 109.5 . . ? H10C C103 H10E 109.5 . . ? H10D C103 H10E 109.5 . . ? C101 C104 H10F 108.2 . . ? C101 C104 H10G 108.2 . . ? C101 C104 H10H 105.9 . . ? C101 C104 H10I 105.9 . . ? H10F C104 H10G 107.4 . . ? H10H C104 H10I 106.2 . . ? C105 C104 C101 116.4(6) . . ? C105 C104 H10F 108.2 . . ? C105 C104 H10G 108.2 . . ? C106 C104 C101 125.8(6) . . ? C106 C104 H10H 105.9 . . ? C106 C104 H10I 105.9 . . ? C104 C105 H10J 109.5 . . ? C104 C105 H10K 109.5 . . ? C104 C105 H10L 109.5 . . ? H10J C105 H10K 109.5 . . ? H10J C105 H10L 109.5 . . ? H10K C105 H10L 109.5 . . ? C104 C106 H10M 109.5 . . ? C104 C106 H10N 109.5 . . ? C104 C106 H10O 109.5 . . ? H10M C106 H10N 109.5 . . ? H10M C106 H10O 109.5 . . ? H10N C106 H10O 109.5 . . ? C20 C201 H201 106.1 . . ? C20 C201 C202 111.4(3) . . ? C20 C201 C204 112.8(3) . . ? C202 C201 H201 106.1 . . ? C202 C201 C204 113.5(3) . . ? C204 C201 H201 106.1 . . ? C201 C202 H20A 109.1 . . ? C201 C202 H20B 109.1 . . ? H20A C202 H20B 107.8 . . ? C203 C202 C201 112.7(3) . . ? C203 C202 H20A 109.1 . . ? C203 C202 H20B 109.1 . . ? C202 C203 H20C 109.5 . . ? C202 C203 H20D 109.5 . . ? C202 C203 H20E 109.5 . . ? H20C C203 H20D 109.5 . . ? H20C C203 H20E 109.5 . . ? H20D C203 H20E 109.5 . . ? C201 C204 H20F 108.9 . . ? C201 C204 H20G 108.9 . . ? H20F C204 H20G 107.8 . . ? C205 C204 C201 113.2(3) . . ? C205 C204 H20F 108.9 . . ? C205 C204 H20G 108.9 . . ? C204 C205 H20H 109.5 . . ? C204 C205 H20I 109.5 . . ? C204 C205 H20J 109.5 . . ? H20H C205 H20I 109.5 . . ? H20H C205 H20J 109.5 . . ? H20I C205 H20J 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Ni1 N22 C6 C7 -174.4(2) . . . . ? Ni1 N22 C6 C5 13.8(5) . . . . ? Ni1 N22 C9 C8 176.5(2) . . . . ? Ni1 N22 C9 C10 2.4(5) . . . . ? Ni1 N23 C11 C10 -12.1(5) . . . . ? Ni1 N23 C11 C12 176.5(2) . . . . ? Ni1 N23 C14 C13 -178.5(2) . . . . ? Ni1 N23 C14 C15 -2.3(5) . . . . ? Ni1 N24 C16 C15 16.7(5) . . . . ? Ni1 N24 C16 C17 -172.2(2) . . . . ? Ni1 N24 C19 C18 174.2(2) . . . . ? Ni1 N24 C19 C20 1.4(5) . . . . ? Ni1 N21 C1 C20 -12.4(5) . . . . ? Ni1 N21 C1 C2 179.1(2) . . . . ? Ni1 N21 C4 C3 178.5(2) . . . . ? Ni1 N21 C4 C5 -6.7(5) . . . . ? N22 C6 C7 C8 -3.3(4) . . . . ? N22 C6 C5 C4 6.9(5) . . . . ? N22 C6 C5 Br1 179.7(2) . . . . ? N22 C9 C10 C11 14.6(5) . . . . ? N22 C9 C10 C101 -172.7(3) . . . . ? N23 C11 C12 C13 3.5(4) . . . . ? N23 C14 C15 C16 -12.4(6) . . . . ? N23 C14 C15 Br2 173.6(2) . . . . ? N24 C16 C17 C18 -4.5(4) . . . . ? N24 C19 C20 C1 16.7(5) . . . . ? N24 C19 C20 C201 -169.9(3) . . . . ? N21 C1 C2 C3 3.4(4) . . . . ? N21 C4 C5 C6 -10.6(5) . . . . ? N21 C4 C5 Br1 176.7(2) . . . . ? C6 N22 C9 C8 0.6(4) . . . . ? C6 N22 C9 C10 -173.5(3) . . . . ? C6 C7 C8 C9 3.5(4) . . . . ? C7 C6 C5 C4 -163.8(3) . . . . ? C7 C6 C5 Br1 9.0(5) . . . . ? C7 C8 C9 N22 -2.7(4) . . . . ? C7 C8 C9 C10 171.4(4) . . . . ? C8 C9 C10 C11 -158.5(3) . . . . ? C8 C9 C10 C101 14.1(6) . . . . ? C9 N22 C6 C7 1.6(4) . . . . ? C9 N22 C6 C5 -170.2(3) . . . . ? C9 C10 C11 N23 -9.7(5) . . . . ? C9 C10 C11 C12 160.4(3) . . . . ? C9 C10 C101 C102 54.5(5) . . . . ? C9 C10 C101 C104 -79.5(5) . . . . ? C10 C11 C12 C13 -167.9(3) . . . . ? C10 C101 C102 C103 56.1(6) . . . . ? C10 C101 C104 C105 -148.6(7) . . . . ? C10 C101 C104 C106 -43.1(10) . . . . ? C11 N23 C14 C13 0.3(4) . . . . ? C11 N23 C14 C15 176.5(3) . . . . ? C11 C10 C101 C102 -132.8(4) . . . . ? C11 C10 C101 C104 93.2(5) . . . . ? C11 C12 C13 C14 -3.2(4) . . . . ? C12 C13 C14 N23 1.9(4) . . . . ? C12 C13 C14 C15 -174.2(3) . . . . ? C13 C14 C15 C16 163.1(4) . . . . ? C13 C14 C15 Br2 -10.9(5) . . . . ? C14 N23 C11 C10 169.1(3) . . . . ? C14 N23 C11 C12 -2.3(4) . . . . ? C14 C15 C16 N24 5.0(6) . . . . ? C14 C15 C16 C17 -164.6(4) . . . . ? C15 C16 C17 C18 166.2(3) . . . . ? C16 N24 C19 C18 -1.6(4) . . . . ? C16 N24 C19 C20 -174.3(3) . . . . ? C16 C17 C18 C19 3.4(4) . . . . ? C17 C18 C19 N24 -1.2(4) . . . . ? C17 C18 C19 C20 171.6(3) . . . . ? C18 C19 C20 C1 -154.8(3) . . . . ? C18 C19 C20 C201 18.5(5) . . . . ? C19 N24 C16 C15 -167.5(3) . . . . ? C19 N24 C16 C17 3.6(4) . . . . ? C19 C20 C1 N21 -11.2(5) . . . . ? C19 C20 C1 C2 155.6(3) . . . . ? C19 C20 C201 C202 56.6(4) . . . . ? C19 C20 C201 C204 -72.4(4) . . . . ? C20 C1 C2 C3 -165.2(3) . . . . ? C20 C201 C202 C203 166.1(3) . . . . ? C20 C201 C204 C205 -128.4(3) . . . . ? C1 N21 C4 C3 -1.1(3) . . . . ? C1 N21 C4 C5 173.7(3) . . . . ? C1 C20 C201 C202 -130.0(3) . . . . ? C1 C20 C201 C204 101.0(4) . . . . ? C1 C2 C3 C4 -3.9(4) . . . . ? C2 C3 C4 N21 3.2(4) . . . . ? C2 C3 C4 C5 -171.5(3) . . . . ? C3 C4 C5 C6 163.4(3) . . . . ? C3 C4 C5 Br1 -9.3(5) . . . . ? C4 N21 C1 C20 167.2(3) . . . . ? C4 N21 C1 C2 -1.3(3) . . . . ? C5 C6 C7 C8 168.4(3) . . . . ? Br2 C15 C16 N24 179.0(2) . . . . ? Br2 C15 C16 C17 9.4(5) . . . . ? C101 C10 C11 N23 177.4(3) . . . . ? C101 C10 C11 C12 -12.4(5) . . . . ? C102 C101 C104 C105 76.9(8) . . . . ? C102 C101 C104 C106 -177.6(8) . . . . ? C104 C101 C102 C103 -171.0(5) . . . . ? C201 C20 C1 N21 175.3(3) . . . . ? C201 C20 C1 C2 -17.9(5) . . . . ? C202 C201 C204 C205 103.7(4) . . . . ? C204 C201 C202 C203 -65.2(4) . . . . ? _shelx_res_file ; TITL cu_ehgdibr_0ma in C2/c he015.res created by SHELXL-2018/1 at 10:44:40 on 11-Jun-2020 CELL 1.54178 44.0507 10.2192 11.8461 90 91.771 90 ZERR 8 0.0016 0.0004 0.0004 0 0.003 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H Br N Ni UNIT 240 240 16 32 8 SIMU 0.001 0.002 2 C106 C105 C104 L.S. 12 PLAN 20 SIZE 0.05 0.1 0.35 TEMP -173 BOND $H WPDB LIST 4 HTAB CONF fmap 2 acta REM REM REM WGHT 0.073600 20.000900 FVAR 0.08681 NI1 5 0.123701 0.242089 0.062983 11.00000 0.01332 0.01028 = 0.00985 0.00140 0.00045 0.00198 N22 4 0.130723 0.114239 0.178447 11.00000 0.01580 0.01318 = 0.01181 -0.00087 0.00126 0.00262 N23 4 0.083020 0.259892 0.111326 11.00000 0.01695 0.01158 = 0.01343 0.00101 0.00007 0.00069 N24 4 0.116065 0.361139 -0.059273 11.00000 0.01532 0.01377 = 0.01239 0.00102 0.00138 0.00252 N21 4 0.164728 0.225866 0.015679 11.00000 0.01604 0.01138 = 0.00973 -0.00069 -0.00003 0.00156 C6 1 0.153139 0.020005 0.180742 11.00000 0.01883 0.01158 = 0.01640 -0.00010 -0.00290 0.00075 C7 1 0.149743 -0.066100 0.274054 11.00000 0.02533 0.01977 = 0.02079 0.00971 0.00040 0.00599 AFIX 43 H7 2 0.161696 -0.141161 0.291696 11.00000 -1.20000 AFIX 0 C8 1 0.126188 -0.019986 0.332461 11.00000 0.02581 0.02631 = 0.02019 0.01183 0.00281 0.00337 AFIX 43 H8 2 0.119174 -0.054399 0.401443 11.00000 -1.20000 AFIX 0 C9 1 0.113660 0.089500 0.272494 11.00000 0.01940 0.01961 = 0.01320 0.00281 0.00019 -0.00090 C10 1 0.086676 0.153530 0.297977 11.00000 0.02006 0.01539 = 0.01468 -0.00019 0.00326 -0.00242 C11 1 0.071634 0.227053 0.215651 11.00000 0.01720 0.01214 = 0.01780 -0.00145 0.00408 -0.00302 C12 1 0.040265 0.263776 0.218784 11.00000 0.01833 0.01668 = 0.02551 0.00266 0.00711 0.00106 AFIX 43 H12 2 0.027581 0.256119 0.281863 11.00000 -1.20000 AFIX 0 C13 1 0.031990 0.311144 0.116128 11.00000 0.01603 0.01841 = 0.02806 0.00480 0.00445 0.00513 AFIX 43 H13 2 0.012237 0.339088 0.092406 11.00000 -1.20000 AFIX 0 C14 1 0.058680 0.311381 0.049391 11.00000 0.01554 0.01167 = 0.02320 -0.00043 0.00190 0.00240 C15 1 0.061016 0.362007 -0.057159 11.00000 0.01576 0.01474 = 0.02229 0.00386 -0.00451 0.00343 C16 1 0.087957 0.390673 -0.108682 11.00000 0.01771 0.01639 = 0.01599 -0.00126 -0.00121 0.00315 C17 1 0.091615 0.469229 -0.206367 11.00000 0.01956 0.02410 = 0.01503 0.00537 -0.00255 0.00669 AFIX 43 H17 2 0.075888 0.497194 -0.257495 11.00000 -1.20000 AFIX 0 C18 1 0.121162 0.496653 -0.213319 11.00000 0.02302 0.01940 = 0.01580 0.00621 -0.00045 0.00389 AFIX 43 H18 2 0.130138 0.551143 -0.268044 11.00000 -1.20000 AFIX 0 C19 1 0.136972 0.428166 -0.122254 11.00000 0.02029 0.01338 = 0.01198 0.00041 0.00147 0.00046 C20 1 0.168120 0.418413 -0.108849 11.00000 0.02062 0.01578 = 0.00751 -0.00118 0.00235 -0.00068 C1 1 0.180729 0.313456 -0.049092 11.00000 0.01606 0.01477 = 0.00934 -0.00132 -0.00025 -0.00091 C2 1 0.211026 0.263680 -0.063133 11.00000 0.01452 0.02109 = 0.01400 -0.00236 0.00188 0.00044 AFIX 43 H2 2 0.226934 0.306784 -0.100711 11.00000 -1.20000 AFIX 0 C3 1 0.212741 0.145645 -0.013664 11.00000 0.01537 0.02092 = 0.01293 -0.00098 0.00146 0.00571 AFIX 43 H3 2 0.229602 0.087675 -0.013409 11.00000 -1.20000 AFIX 0 C4 1 0.184217 0.123665 0.038834 11.00000 0.01563 0.01525 = 0.01225 -0.00369 -0.00117 0.00234 C5 1 0.177714 0.021634 0.110442 11.00000 0.01763 0.01411 = 0.01320 -0.00261 -0.00224 0.00449 BR2 3 0.024366 0.411008 -0.134079 11.00000 0.01629 0.05214 = 0.03525 0.02147 -0.00337 0.00609 BR1 3 0.206463 -0.115681 0.125916 11.00000 0.02597 0.01862 = 0.02314 0.00424 0.00248 0.01147 C101 1 0.071411 0.130734 0.411137 11.00000 0.02671 0.03192 = 0.01972 0.00475 0.00871 0.00363 AFIX 13 H101 2 0.055618 0.200836 0.414133 11.00000 -1.20000 AFIX 0 C102 1 0.091263 0.153566 0.515502 11.00000 0.05098 0.05935 = 0.02273 -0.00005 0.00522 0.01387 AFIX 23 H10A 2 0.078860 0.139149 0.582665 11.00000 -1.20000 H10B 2 0.107625 0.087121 0.517356 11.00000 -1.20000 AFIX 0 C103 1 0.105302 0.283817 0.524927 11.00000 0.08015 0.06903 = 0.02901 -0.00180 -0.00393 -0.00897 AFIX 137 H10C 2 0.117928 0.288388 0.594393 11.00000 -1.50000 H10D 2 0.089380 0.350673 0.527043 11.00000 -1.50000 H10E 2 0.117955 0.299195 0.459625 11.00000 -1.50000 AFIX 0 C104 1 0.053312 0.003463 0.412110 11.00000 0.05728 0.04854 = 0.06250 0.01502 0.01643 -0.02102 PART 1 AFIX 23 H10F 2 0.046833 -0.017446 0.333397 10.50000 -1.20000 H10G 2 0.067049 -0.067493 0.438796 10.50000 -1.20000 AFIX 23 PART 0 PART 2 H10H 2 0.068350 -0.066892 0.427123 10.50000 -1.20000 H10I 2 0.040656 0.008014 0.479619 10.50000 -1.20000 AFIX 0 PART 0 PART 1 C105 1 0.026421 0.002282 0.481451 10.50000 0.05862 0.04931 = 0.06467 0.01576 0.01465 -0.01984 AFIX 137 H10J 2 0.013444 0.077134 0.461308 10.50000 -1.50000 H10K 2 0.032691 0.008034 0.561394 10.50000 -1.50000 H10L 2 0.015106 -0.079114 0.468124 10.50000 -1.50000 AFIX 0 PART 0 PART 2 C106 1 0.034311 -0.042281 0.325167 10.50000 0.05849 0.04817 = 0.06394 0.01655 0.01367 -0.02171 AFIX 137 H10M 2 0.028372 -0.132682 0.341064 10.50000 -1.50000 H10N 2 0.045019 -0.039292 0.253917 10.50000 -1.50000 H10O 2 0.016128 0.012833 0.319133 10.50000 -1.50000 AFIX 0 PART 0 C201 1 0.189268 0.512626 -0.169138 11.00000 0.01697 0.01466 = 0.01663 0.00141 0.00116 -0.00093 AFIX 13 H201 2 0.210179 0.494879 -0.137561 11.00000 -1.20000 AFIX 0 C202 1 0.182248 0.656175 -0.140064 11.00000 0.02514 0.01626 = 0.02052 0.00209 0.00153 -0.00119 AFIX 23 H20A 2 0.162917 0.682020 -0.178686 11.00000 -1.20000 H20B 2 0.179527 0.663787 -0.057680 11.00000 -1.20000 AFIX 0 C203 1 0.207273 0.749853 -0.174728 11.00000 0.03064 0.01671 = 0.02574 0.00429 0.00250 -0.00379 AFIX 137 H20C 2 0.202033 0.839165 -0.152342 11.00000 -1.50000 H20D 2 0.209336 0.746247 -0.256804 11.00000 -1.50000 H20E 2 0.226521 0.724313 -0.137302 11.00000 -1.50000 AFIX 0 C204 1 0.190433 0.485874 -0.298676 11.00000 0.02590 0.01992 = 0.01336 0.00207 0.00384 -0.00094 AFIX 23 H20F 2 0.179034 0.404593 -0.316500 11.00000 -1.20000 H20G 2 0.180210 0.558627 -0.339869 11.00000 -1.20000 AFIX 0 C205 1 0.222509 0.472092 -0.340035 11.00000 0.02694 0.02866 = 0.01990 0.00047 0.00533 -0.00339 AFIX 137 H20H 2 0.221808 0.455057 -0.421486 11.00000 -1.50000 H20I 2 0.232668 0.399151 -0.300676 11.00000 -1.50000 H20J 2 0.233780 0.553160 -0.324674 11.00000 -1.50000 AFIX 0 HKLF 4 REM cu_ehgdibr_0ma in C2/c REM R1 = 0.0443 for 4210 Fo > 4sig(Fo) and 0.0476 for all 4611 data REM 348 parameters refined using 18 restraints END WGHT 0.0736 20.0180 REM Instructions for potential hydrogen bonds EQIV $1 -x, -y+1, -z HTAB C13 Br2_$1 REM Highest difference peak 1.169, deepest hole -1.530, 1-sigma level 0.121 Q1 1 0.0262 0.3427 -0.1726 11.00000 0.05 1.17 Q2 1 0.2308 -0.1148 0.1258 11.00000 0.05 1.01 Q3 1 0.0722 0.2389 0.4930 11.00000 0.05 0.96 Q4 1 0.1833 -0.1152 0.1326 11.00000 0.05 0.95 Q5 1 0.0751 0.2093 0.6215 11.00000 0.05 0.88 Q6 1 0.0474 0.4154 -0.1378 11.00000 0.05 0.85 Q7 1 0.0008 0.4053 -0.1288 11.00000 0.05 0.78 Q8 1 0.1482 0.2409 0.0598 11.00000 0.05 0.77 Q9 1 0.0249 -0.0138 0.3687 11.00000 0.05 0.73 Q10 1 0.0995 0.2451 0.0724 11.00000 0.05 0.70 Q11 1 0.0435 -0.0631 0.3018 11.00000 0.05 0.59 Q12 1 0.1901 -0.2228 0.1644 11.00000 0.05 0.53 Q13 1 0.0109 0.5228 -0.0872 11.00000 0.05 0.52 Q14 1 0.2218 -0.2234 0.0817 11.00000 0.05 0.51 Q15 1 0.0111 0.3206 -0.0769 11.00000 0.05 0.50 Q16 1 0.0381 0.5218 -0.1877 11.00000 0.05 0.50 Q17 1 0.0394 0.0618 0.4117 11.00000 0.05 0.45 Q18 1 0.2226 -0.0169 0.0904 11.00000 0.05 0.43 Q19 1 0.1894 -0.0095 0.1482 11.00000 0.05 0.43 Q20 1 0.1670 0.0060 0.1467 11.00000 0.05 0.41 ; _shelx_res_checksum 70037 _shelx_hkl_file ; 2 0 0 0.17 0.07 -2 0 0 0.16 0.06 4 0 0 336.44 1.85 6 0 0 87.55 1.20 8 0 0 303.48 2.55 10 0 0 814.75 4.69 10 0 0 891.50 4.87 12 0 0 1850.05 7.72 12 0 0 1952.66 7.96 14 0 0 0.05 0.48 14 0 0 0.41 0.44 16 0 0 26.37 1.37 16 0 0 26.68 1.31 18 0 0 332.80 4.18 18 0 0 335.75 4.29 20 0 0 1023.64 7.66 20 0 0 991.64 7.85 22 0 0 731.41 6.89 24 0 0 266.12 4.48 26 0 0 275.13 4.78 28 0 0 135.74 3.88 28 0 0 120.42 3.45 28 0 0 133.34 3.29 30 0 0 51.39 2.70 30 0 0 47.70 2.52 30 0 0 50.50 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6 14.99 2.02 22 2 6 15.14 1.71 24 2 6 18.76 1.80 24 2 6 22.94 1.96 26 2 6 100.56 3.67 26 2 6 142.20 3.78 28 2 6 0.63 0.77 28 2 6 1.04 0.95 30 2 6 5.70 1.30 30 2 6 7.31 1.33 32 2 6 135.60 4.28 34 2 6 90.19 3.50 36 2 6 2.73 1.00 38 2 6 27.22 1.98 -38 -2 -6 29.04 2.44 40 2 6 1.01 0.73 -40 -2 -6 1.37 0.99 42 2 6 6.18 0.99 -42 -2 -6 6.03 1.31 44 2 6 13.04 1.04 -44 -2 -6 13.56 1.61 48 -2 -5 0.56 0.77 46 -2 -5 143.58 3.96 44 -2 -5 13.32 1.82 42 -2 -5 19.75 2.16 40 -2 -5 171.47 5.18 38 -2 -5 9.90 1.81 38 -2 -5 10.24 1.55 36 -2 -5 101.34 4.29 36 -2 -5 109.13 3.66 34 -2 -5 59.80 3.53 34 -2 -5 62.93 3.06 -32 2 5 1.52 1.19 32 -2 -5 1.69 1.35 32 -2 -5 0.48 1.06 -30 2 5 20.03 2.49 30 -2 -5 18.35 2.29 30 -2 -5 19.54 2.19 -28 2 5 393.62 7.77 28 -2 -5 387.23 7.58 28 -2 -5 413.31 6.99 -26 2 5 10.97 1.89 26 -2 -5 13.57 2.13 26 -2 -5 12.76 1.81 -24 2 5 318.25 6.59 24 -2 -5 338.80 6.77 24 -2 -5 443.63 6.99 22 -2 -5 19.78 2.11 22 -2 -5 23.50 2.11 20 -2 -5 12.53 1.71 -16 2 5 10.32 1.57 -14 2 5 37.54 2.16 -12 2 5 67.55 2.59 -10 2 5 18.58 1.64 -8 2 5 253.90 4.29 -6 2 5 622.23 6.41 -4 2 5 8.29 1.10 -2 2 5 1509.52 9.52 -2 2 5 1437.27 9.65 0 2 5 43.49 1.86 0 2 5 45.52 1.88 2 2 5 20.05 1.42 2 2 5 17.96 1.31 4 2 5 311.47 4.31 4 2 5 298.89 4.46 6 2 5 164.22 3.22 6 2 5 155.59 3.30 8 2 5 191.24 3.49 8 2 5 177.77 3.59 10 2 5 759.91 6.85 10 2 5 718.33 7.24 12 2 5 57.72 2.14 12 2 5 52.30 2.17 -12 -2 -5 62.77 2.32 14 2 5 12.30 1.36 -14 -2 -5 11.31 1.43 16 2 5 886.69 7.87 18 2 5 33.88 1.92 20 2 5 361.10 5.96 20 2 5 360.92 6.02 20 2 5 423.04 5.75 22 2 5 42.83 2.28 22 2 5 45.72 2.45 22 2 5 48.92 2.28 24 2 5 56.90 2.65 24 2 5 60.51 2.85 24 2 5 74.17 2.72 26 2 5 28.28 2.08 26 2 5 30.07 2.26 26 2 5 42.02 2.25 28 2 5 21.75 1.93 28 2 5 22.78 2.18 28 2 5 30.14 2.04 30 2 5 10.06 1.59 30 2 5 7.59 1.57 30 2 5 10.38 1.48 32 2 5 85.70 3.43 32 2 5 82.43 3.90 32 2 5 92.01 2.86 34 2 5 8.08 1.47 36 2 5 225.03 5.25 38 2 5 67.20 2.93 40 2 5 15.45 1.60 42 2 5 116.75 3.20 44 2 5 23.72 1.43 -44 -2 -5 25.16 2.05 -46 -2 -5 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0.79 12 2 4 4.23 0.79 -12 -2 -4 5.09 0.92 14 2 4 11.03 1.23 14 2 4 10.60 1.16 -14 -2 -4 10.53 1.32 16 2 4 18.12 1.39 16 2 4 18.66 1.42 18 2 4 19.32 1.48 18 2 4 19.34 1.51 20 2 4 108.10 2.83 20 2 4 111.89 3.38 22 2 4 0.59 0.60 22 2 4 0.43 0.68 22 2 4 0.43 0.67 24 2 4 0.70 0.70 24 2 4 1.03 0.76 24 2 4 0.93 0.76 26 2 4 249.79 5.14 26 2 4 304.04 5.83 26 2 4 387.66 5.45 28 2 4 -0.29 0.59 28 2 4 -0.09 0.73 28 2 4 0.86 0.83 30 2 4 131.54 4.02 30 2 4 131.62 4.22 30 2 4 150.14 3.54 32 2 4 0.34 0.74 32 2 4 -0.26 0.76 32 2 4 0.90 0.76 34 2 4 8.02 1.48 34 2 4 8.12 1.65 36 2 4 0.66 0.77 36 2 4 -0.44 0.94 38 2 4 44.16 2.52 40 2 4 2.06 0.90 42 2 4 1.93 0.82 44 2 4 19.77 1.48 46 2 4 37.99 1.48 50 -2 -3 28.39 1.84 48 -2 -3 15.96 1.74 46 -2 -3 17.87 2.03 44 -2 -3 56.55 3.11 42 -2 -3 194.06 5.53 40 -2 -3 4.23 1.49 40 -2 -3 4.71 1.26 38 -2 -3 21.72 2.45 38 -2 -3 21.74 2.16 36 -2 -3 104.03 4.30 36 -2 -3 121.79 3.98 34 -2 -3 11.35 1.92 34 -2 -3 15.62 2.00 -32 2 3 400.29 7.92 32 -2 -3 388.21 7.61 32 -2 -3 457.75 7.29 -30 2 3 30.41 2.66 30 -2 -3 27.97 2.48 30 -2 -3 34.83 2.41 -28 2 3 174.11 4.99 28 -2 -3 167.12 4.82 28 -2 -3 201.59 4.79 26 -2 -3 1.37 1.01 26 -2 -3 -0.07 0.91 24 -2 -3 38.24 2.25 -20 2 3 495.96 6.62 -18 2 3 89.92 2.85 -16 2 3 305.15 4.67 -14 2 3 390.84 4.98 -12 2 3 24.69 1.51 -12 2 3 23.01 1.38 -10 2 3 977.13 6.99 -10 2 3 914.03 6.85 -8 2 3 118.58 2.45 -8 2 3 112.44 2.38 -6 2 3 312.18 3.64 -6 2 3 303.87 3.64 -4 2 3 3.70 0.71 -4 2 3 3.21 0.56 -2 2 3 64.97 1.65 -2 2 3 64.03 1.64 0 2 3 51.36 1.46 0 2 3 48.94 1.43 2 2 3 710.20 4.75 2 2 3 685.91 4.91 4 2 3 96.38 1.86 4 2 3 93.47 1.91 6 2 3 1392.57 6.68 6 2 3 1390.41 7.21 8 2 3 24.45 1.15 8 2 3 23.00 1.14 10 2 3 9.20 0.95 10 2 3 9.50 0.91 12 2 3 862.55 5.80 12 2 3 894.73 6.57 -12 -2 -3 1046.93 7.87 14 2 3 9.45 1.08 14 2 3 10.49 1.04 -14 -2 -3 12.47 1.27 16 2 3 463.33 4.66 16 2 3 523.08 5.62 18 2 3 190.88 3.21 18 2 3 208.61 3.82 20 2 3 68.18 2.14 20 2 3 70.44 2.45 22 2 3 34.25 1.73 22 2 3 31.03 1.87 24 2 3 329.39 5.37 24 2 3 421.57 6.19 24 2 3 515.13 5.72 26 2 3 4.93 1.10 26 2 3 5.86 1.25 26 2 3 5.80 1.08 28 2 3 329.86 5.82 28 2 3 358.84 6.28 28 2 3 390.50 5.25 30 2 3 9.09 1.41 30 2 3 7.81 1.46 30 2 3 9.89 1.31 32 2 3 44.71 2.50 32 2 3 48.91 2.81 34 2 3 155.49 4.36 34 2 3 145.53 4.55 36 2 3 21.05 1.97 36 2 3 23.28 2.30 38 2 3 38.47 2.40 38 2 3 34.01 2.64 40 2 3 65.11 2.83 40 2 3 64.28 3.33 42 2 3 7.23 1.25 44 2 3 58.79 2.32 46 2 3 92.19 2.38 50 -2 -2 33.18 2.01 48 -2 -2 32.46 2.24 46 -2 -2 21.22 2.15 44 -2 -2 3.25 1.28 42 -2 -2 97.80 4.15 40 -2 -2 2.65 1.24 40 -2 -2 2.68 1.13 38 -2 -2 3.03 1.38 38 -2 -2 4.38 1.26 36 -2 -2 21.27 2.38 36 -2 -2 26.68 2.35 -34 2 2 -0.81 1.14 34 -2 -2 0.13 0.82 34 -2 -2 -0.01 1.01 -32 2 2 82.16 3.84 32 -2 -2 79.77 3.70 32 -2 -2 90.50 3.51 -30 2 2 385.63 7.35 30 -2 -2 394.20 7.33 30 -2 -2 458.33 7.08 -28 2 2 172.52 4.87 28 -2 -2 155.14 4.56 28 -2 -2 194.70 4.63 26 -2 -2 80.79 3.00 24 -2 -2 7.04 1.32 -20 2 2 118.68 3.27 -18 2 2 260.97 4.38 -16 2 2 146.34 3.17 -14 2 2 48.50 1.84 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0.54 0.74 38 2 2 1.19 1.00 40 2 2 41.17 2.36 40 2 2 37.33 2.70 42 2 2 18.59 1.72 42 2 2 14.76 2.05 44 2 2 77.64 2.68 46 2 2 0.82 0.58 50 -2 -1 54.19 2.47 48 -2 -1 1.23 0.96 46 -2 -1 262.36 5.95 44 -2 -1 57.78 3.22 42 -2 -1 9.69 1.81 42 -2 -1 10.56 1.73 40 -2 -1 66.28 3.58 40 -2 -1 68.97 3.05 38 -2 -1 10.83 1.89 38 -2 -1 11.01 1.75 36 -2 -1 344.61 7.39 36 -2 -1 406.88 6.97 -34 2 1 158.47 5.15 34 -2 -1 148.24 4.89 34 -2 -1 181.23 4.76 -32 2 1 45.43 3.05 32 -2 -1 42.99 2.86 32 -2 -1 52.71 2.82 -30 2 1 18.11 2.32 30 -2 -1 19.87 1.94 28 -2 -1 654.50 8.94 28 -2 -1 806.20 8.97 26 -2 -1 -0.40 0.73 -22 2 1 2.18 0.99 -20 2 1 116.81 3.15 -16 2 1 235.91 3.77 -14 2 1 76.37 2.14 -10 2 1 17.55 1.12 -8 2 1 166.84 2.36 -6 2 1 420.84 3.28 -6 2 1 412.26 3.36 6 -2 -1 371.37 3.51 -4 2 1 46.08 1.11 -4 2 1 48.39 1.12 4 -2 -1 39.95 1.21 -2 2 1 2117.58 5.54 2 -2 -1 1955.34 7.35 0 -2 -1 205.32 2.33 2 2 1 30.59 0.70 -2 -2 -1 28.87 0.94 4 2 1 609.35 2.73 -4 -2 -1 523.41 3.34 6 2 1 734.25 3.30 8 2 1 409.62 2.80 10 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0.86 34 -2 0 1.05 1.11 34 -2 0 0.39 0.95 -32 2 0 2.14 1.19 32 -2 0 2.82 1.24 32 -2 0 3.08 1.15 -30 2 0 5.63 1.36 30 -2 0 6.05 1.45 30 -2 0 6.05 1.30 28 -2 0 0.90 0.94 28 -2 0 1.74 0.92 26 -2 0 23.82 1.82 -22 2 0 4.62 1.07 -20 2 0 19.44 1.64 -16 2 0 87.46 2.39 -14 2 0 20.95 1.32 14 -2 0 27.59 1.23 -12 2 0 8.83 1.01 12 -2 0 10.87 0.89 -10 2 0 13.80 1.02 -8 2 0 1.67 0.52 -8 2 0 2.23 0.50 -6 2 0 367.58 2.89 -6 2 0 385.12 3.08 -4 2 0 169.49 1.70 -4 2 0 192.57 1.91 -4 2 0 131.74 1.54 -2 2 0 7.72 0.47 -2 2 0 5.53 0.60 0 2 0 0.03 0.36 2 2 0 6.16 0.74 4 2 0 145.92 2.11 6 2 0 332.89 3.26 8 2 0 2.43 0.34 10 2 0 18.36 0.76 -10 -2 0 22.13 1.15 12 2 0 11.13 0.76 14 2 0 29.67 1.14 16 2 0 114.48 2.22 18 2 0 89.56 1.78 18 2 0 101.23 2.30 20 2 0 20.02 1.13 20 2 0 25.43 1.44 22 2 0 5.56 0.78 22 2 0 6.37 0.97 24 2 0 391.79 4.23 24 2 0 427.71 5.65 26 2 0 19.02 1.64 26 2 0 19.48 1.29 28 2 0 0.72 0.67 28 2 0 1.23 0.81 28 2 0 1.11 0.74 28 2 0 1.33 0.84 30 2 0 5.67 1.09 30 2 0 5.59 1.23 30 2 0 4.97 1.21 32 2 0 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3 -7 363.43 4.91 3 3 -7 408.70 6.98 -3 -3 7 344.64 6.06 5 3 -7 38.20 2.11 5 3 -7 37.90 2.22 5 3 -7 39.67 1.84 5 3 -7 44.38 2.70 7 3 -7 11.95 1.48 7 3 -7 12.32 1.58 7 3 -7 15.00 1.34 7 3 -7 12.82 1.88 9 3 -7 314.65 5.38 9 3 -7 322.96 5.67 9 3 -7 306.76 4.17 9 3 -7 357.35 6.65 11 3 -7 68.86 2.73 11 3 -7 67.52 2.84 11 3 -7 74.74 3.32 13 3 -7 34.78 2.08 13 3 -7 41.19 2.66 15 3 -7 17.54 1.73 15 3 -7 22.29 2.32 17 3 -7 695.00 8.00 17 3 -7 716.24 9.57 17 3 -7 578.14 8.79 19 3 -7 146.65 3.86 19 3 -7 147.52 4.62 19 3 -7 108.02 4.21 21 3 -7 101.79 3.32 21 3 -7 101.89 4.01 21 3 -7 84.40 4.21 23 3 -7 9.93 1.43 23 3 -7 10.80 2.04 25 3 -7 15.22 1.69 27 3 -7 20.19 1.77 29 3 -7 124.24 3.42 29 3 -7 121.61 4.32 29 3 -7 157.37 5.12 31 3 -7 28.23 1.84 31 3 -7 28.14 2.59 31 3 -7 35.66 3.01 33 3 -7 0.53 0.71 33 3 -7 -0.13 1.07 35 3 -7 56.94 3.11 35 3 -7 67.52 3.34 37 3 -7 57.36 3.00 37 3 -7 66.48 3.19 39 3 -7 127.46 3.99 39 3 -7 139.50 4.09 41 3 -7 12.37 1.67 41 3 -7 14.49 1.67 -39 3 -8 20.16 1.74 39 -3 8 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22 4 5 6.48 1.26 24 4 5 41.94 2.04 24 4 5 48.06 2.58 26 4 5 0.90 0.64 26 4 5 1.99 0.96 28 4 5 4.68 0.96 28 4 5 6.01 1.37 30 4 5 9.66 1.23 30 4 5 10.64 1.70 32 4 5 47.90 2.00 32 4 5 54.23 2.94 34 4 5 13.81 1.32 34 4 5 16.01 1.97 36 4 5 34.43 2.50 38 4 5 40.16 2.60 40 4 5 52.87 2.73 42 4 5 14.42 1.73 -44 -4 -5 8.71 1.43 -46 4 4 80.80 3.09 46 -4 -4 71.62 2.95 -44 4 4 135.84 4.21 44 -4 -4 123.15 4.04 -42 4 4 62.14 3.24 42 -4 -4 56.48 3.13 42 -4 -4 62.39 2.72 -40 4 4 6.82 1.56 40 -4 -4 7.78 1.78 40 -4 -4 8.46 1.60 -38 4 4 2.16 1.21 38 -4 -4 1.17 1.19 38 -4 -4 1.87 1.22 -36 4 4 0.30 1.06 36 -4 -4 -0.22 1.05 36 -4 -4 -0.11 1.18 -34 4 4 245.26 6.42 34 -4 -4 195.82 6.34 34 -4 -4 259.74 6.16 -32 4 4 53.65 3.35 32 -4 -4 52.42 3.22 -30 4 4 4.23 1.38 -30 4 4 3.86 1.51 30 -4 -4 4.32 1.60 -28 4 4 5.94 1.58 -28 4 4 4.40 1.45 28 -4 -4 5.70 1.59 -26 4 4 6.98 1.42 -26 4 4 5.40 1.48 26 -4 -4 7.47 1.71 -24 4 4 25.21 2.32 -24 4 4 21.28 2.27 24 -4 -4 30.54 2.56 -22 4 4 964.91 10.85 -22 4 4 903.20 9.82 22 -4 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3.03 34 4 4 0.26 0.87 36 4 4 90.75 3.59 38 4 4 97.74 3.69 40 4 4 31.06 2.31 42 4 4 0.24 0.83 44 4 4 75.02 2.87 -46 4 3 1.13 0.95 46 -4 -3 1.77 0.97 -44 4 3 12.58 1.97 44 -4 -3 10.30 1.76 44 -4 -3 11.04 1.51 -42 4 3 34.95 2.63 42 -4 -3 28.50 2.52 42 -4 -3 33.08 2.30 -40 4 3 14.17 2.03 40 -4 -3 15.71 2.28 40 -4 -3 18.27 2.14 -38 4 3 30.66 2.70 38 -4 -3 23.40 2.57 38 -4 -3 29.04 2.56 -36 4 3 94.04 4.15 36 -4 -3 83.85 4.09 36 -4 -3 107.00 4.10 -34 4 3 43.71 3.13 34 -4 -3 44.89 3.05 -32 4 3 103.44 4.29 -32 4 3 74.81 3.82 32 -4 -3 111.31 4.29 -30 4 3 19.10 2.36 -30 4 3 11.98 2.05 30 -4 -3 16.94 2.27 -28 4 3 78.21 3.61 -28 4 3 46.40 2.99 28 -4 -3 76.90 3.60 -26 4 3 1.60 0.99 -26 4 3 0.83 1.09 26 -4 -3 1.66 1.17 -24 4 3 61.96 3.04 -24 4 3 45.23 2.70 24 -4 -3 62.88 3.16 -22 4 3 1.40 0.93 -22 4 3 0.58 0.92 22 -4 -3 0.91 1.08 -20 4 3 68.93 2.98 -20 4 3 66.07 2.75 20 -4 -3 77.93 3.12 -18 4 3 180.63 3.99 -16 4 3 199.94 3.96 -14 4 3 32.72 1.81 -14 4 3 21.14 1.57 -12 4 3 3.49 0.86 -12 4 3 2.83 0.76 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43.77 2.74 44 -4 -2 40.89 2.73 44 -4 -2 44.41 2.38 -42 4 2 83.76 3.74 42 -4 -2 74.93 3.64 42 -4 -2 86.79 3.37 -40 4 2 43.99 2.99 40 -4 -2 36.66 2.88 40 -4 -2 44.84 2.82 -38 4 2 27.65 2.64 38 -4 -2 24.63 2.62 38 -4 -2 28.97 2.55 -36 4 2 4.86 1.53 36 -4 -2 4.81 1.54 36 -4 -2 7.20 1.70 -34 4 2 10.18 1.81 34 -4 -2 10.33 1.86 -32 4 2 7.06 1.64 -32 4 2 4.56 1.68 32 -4 -2 8.15 1.77 -30 4 2 365.67 7.38 -30 4 2 259.32 6.05 30 -4 -2 385.59 7.25 -28 4 2 13.74 1.96 -28 4 2 9.99 1.79 28 -4 -2 15.47 2.13 -26 4 2 243.38 5.69 -26 4 2 138.49 4.20 26 -4 -2 234.59 5.48 -24 4 2 11.70 1.73 -24 4 2 6.35 1.37 24 -4 -2 9.05 1.67 -22 4 2 97.72 3.45 -22 4 2 75.81 2.96 22 -4 -2 93.27 3.44 -20 4 2 196.71 4.20 20 -4 -2 225.13 4.82 -18 4 2 735.69 7.40 -16 4 2 72.04 2.41 -14 4 2 280.84 4.12 -12 4 2 4.12 0.86 -10 4 2 32.86 1.49 -8 4 2 1184.95 6.56 -6 4 2 176.16 2.36 -4 4 2 328.75 3.69 -4 4 2 305.33 3.62 -2 4 2 183.42 2.64 0 4 2 8.42 0.78 2 4 2 76.27 1.60 4 4 2 1120.65 5.73 6 4 2 445.32 3.64 8 4 2 21.17 1.00 10 4 2 6.38 0.73 12 4 2 111.45 2.13 14 4 2 535.15 4.81 -14 -4 -2 654.73 7.39 16 4 2 160.70 2.87 -16 -4 -2 193.01 4.26 18 4 2 422.67 4.86 18 4 2 541.83 5.52 18 4 2 546.29 7.05 -18 -4 -2 686.74 8.17 20 4 2 0.02 0.51 20 4 2 0.30 0.51 20 4 2 0.27 0.77 22 4 2 13.70 1.33 22 4 2 12.42 1.27 22 4 2 17.13 1.86 24 4 2 72.26 2.26 24 4 2 89.93 2.80 24 4 2 78.75 2.66 26 4 2 29.68 1.46 26 4 2 42.33 2.19 26 4 2 35.84 2.05 28 4 2 294.06 5.38 28 4 2 247.90 5.05 30 4 2 405.20 6.54 30 4 2 311.83 5.90 32 4 2 9.45 1.53 34 4 2 34.91 2.41 36 4 2 25.26 2.17 38 4 2 0.67 0.89 40 4 2 281.36 5.82 42 4 2 80.13 3.22 44 4 2 1.33 0.88 46 4 2 0.11 0.80 -48 4 1 6.44 1.29 48 -4 -1 6.66 1.29 -46 4 1 20.27 2.00 46 -4 -1 19.82 2.05 46 -4 -1 20.68 1.68 -44 4 1 112.38 4.09 44 -4 -1 99.85 3.97 44 -4 -1 116.54 3.53 -42 4 1 3.72 1.25 42 -4 -1 2.44 1.33 42 -4 -1 5.30 1.45 -40 4 1 0.36 0.96 40 -4 -1 1.09 1.13 40 -4 -1 1.42 1.15 -38 4 1 -0.06 0.98 38 -4 -1 -0.35 1.15 38 -4 -1 0.52 1.16 -36 4 1 11.25 1.98 36 -4 -1 10.88 1.97 -34 4 1 14.43 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1.48 46 -4 1 5.26 1.21 46 -4 1 6.84 1.16 -44 4 -1 -0.38 0.91 44 -4 1 -0.28 0.90 44 -4 1 0.78 0.89 -42 4 -1 19.64 2.24 42 -4 1 16.26 2.20 42 -4 1 20.32 2.06 -40 4 -1 35.00 2.75 40 -4 1 30.32 2.74 40 -4 1 35.81 2.61 -38 4 -1 26.96 2.56 38 -4 1 25.37 2.80 38 -4 1 30.73 2.63 -36 4 -1 234.60 6.24 -36 4 -1 158.65 5.95 36 -4 1 272.78 6.32 -34 4 -1 43.18 2.98 34 -4 1 48.30 3.08 -32 4 -1 34.43 2.69 32 -4 1 41.34 2.94 -30 4 -1 12.37 2.07 -30 4 -1 9.29 1.78 30 -4 1 13.00 2.09 -28 4 -1 33.01 2.49 -28 4 -1 30.65 2.47 28 -4 1 39.80 2.77 -26 4 -1 22.85 2.11 -26 4 -1 18.50 2.02 26 -4 1 25.82 2.27 -24 4 -1 21.24 1.95 -24 4 -1 20.22 1.94 24 -4 1 25.43 2.20 -22 4 -1 16.06 1.71 -22 4 -1 13.95 1.64 22 -4 1 17.32 1.91 -20 4 -1 165.23 3.72 20 -4 1 166.40 3.81 -18 4 -1 16.26 1.49 18 -4 1 20.70 1.54 -16 4 -1 137.33 3.00 16 -4 1 171.68 3.68 -14 4 -1 266.52 3.77 -12 4 -1 49.22 1.65 -10 4 -1 149.21 2.38 -8 4 -1 5.30 0.75 -6 4 -1 50.52 1.47 -6 4 -1 47.90 1.56 -4 4 -1 61.95 1.47 -4 4 -1 54.94 1.72 -2 4 -1 34.19 1.03 -2 4 -1 25.86 1.37 0 4 -1 91.71 2.29 0 -4 1 149.43 2.52 2 4 -1 149.23 2.94 -2 -4 1 202.70 3.00 4 4 -1 6.75 0.98 6 4 -1 42.92 1.87 8 4 -1 71.02 2.36 10 4 -1 82.80 2.57 -10 -4 1 116.28 2.58 -12 -4 1 99.55 2.53 16 4 -1 1.20 0.46 18 4 -1 42.65 1.47 18 4 -1 56.77 2.53 20 4 -1 18.47 1.17 20 4 -1 20.00 1.34 20 4 -1 21.64 1.84 22 4 -1 49.41 1.84 22 4 -1 58.58 2.06 24 4 -1 114.29 2.88 24 4 -1 102.28 2.73 24 4 -1 129.24 3.10 26 4 -1 11.83 1.35 26 4 -1 10.09 1.23 26 4 -1 13.15 1.52 28 4 -1 124.10 3.39 28 4 -1 102.33 3.11 28 4 -1 133.86 3.53 30 4 -1 1.60 0.88 30 4 -1 1.59 0.83 30 4 -1 2.52 0.96 32 4 -1 2.81 1.05 32 4 -1 3.93 1.15 34 4 -1 12.70 1.74 34 4 -1 16.25 1.91 36 4 -1 7.53 1.54 38 4 -1 0.53 0.96 40 4 -1 1.26 0.95 42 4 -1 4.65 1.30 44 4 -1 107.49 3.52 46 4 -1 21.28 1.86 48 4 -1 7.47 1.21 -48 4 -2 6.57 1.23 -46 4 -2 1.20 0.90 46 -4 2 0.78 0.90 46 -4 2 2.39 0.92 -44 4 -2 1.44 1.01 44 -4 2 0.15 0.85 44 -4 2 1.59 0.91 -42 4 -2 87.47 3.73 42 -4 2 74.39 3.58 42 -4 2 86.97 3.31 -40 4 -2 300.93 6.79 40 -4 2 265.09 6.54 40 -4 2 322.53 6.37 -38 4 -2 0.10 0.90 38 -4 2 -0.14 0.97 -36 4 -2 24.12 2.46 36 -4 2 26.78 2.53 -34 4 -2 39.49 2.85 -34 4 -2 30.18 2.82 34 -4 2 45.80 3.09 -32 4 -2 9.29 1.90 -32 4 -2 7.17 1.70 32 -4 2 10.36 1.84 -30 4 -2 457.13 8.16 -30 4 -2 386.86 7.14 30 -4 2 507.97 8.31 -28 4 -2 311.20 6.57 -28 4 -2 296.70 6.07 28 -4 2 381.67 7.07 -26 4 -2 45.07 2.67 -26 4 -2 42.21 2.59 26 -4 2 49.13 2.86 -24 4 -2 104.50 3.66 -24 4 -2 102.84 3.44 24 -4 2 117.89 3.92 -22 4 -2 15.01 1.75 -22 4 -2 15.15 1.72 22 -4 2 18.48 2.00 -20 4 -2 -0.06 0.75 20 -4 2 -0.74 0.84 20 -4 2 0.67 0.65 -18 4 -2 480.29 5.89 -16 4 -2 118.96 2.88 -14 4 -2 340.06 4.36 -12 4 -2 84.39 2.13 -10 4 -2 5.13 0.78 -10 4 -2 5.06 0.76 -8 4 -2 17.39 1.13 -6 4 -2 303.35 3.86 -4 4 -2 1094.32 6.40 -4 4 -2 618.18 5.60 -2 4 -2 80.73 1.67 -2 4 -2 54.97 1.90 0 4 -2 8.68 0.68 0 4 -2 7.69 1.08 2 4 -2 191.04 2.13 2 4 -2 153.08 3.09 -2 -4 2 195.21 3.26 4 4 -2 285.85 4.26 -4 -4 2 369.69 4.56 6 4 -2 149.94 3.25 8 4 -2 1031.17 8.38 10 4 -2 27.36 1.78 12 4 -2 3.66 0.99 14 4 -2 257.20 4.65 16 4 -2 74.92 2.84 16 4 -2 67.59 2.66 18 4 -2 751.89 8.58 20 4 -2 204.85 3.43 22 4 -2 96.01 2.62 22 4 -2 87.53 3.29 24 4 -2 11.73 1.43 26 4 -2 241.17 4.48 28 4 -2 12.17 1.45 28 4 -2 17.02 1.71 30 4 -2 299.44 5.44 30 4 -2 328.60 5.67 32 4 -2 6.80 1.38 32 4 -2 7.11 1.32 34 4 -2 8.60 1.54 34 4 -2 9.22 1.53 36 4 -2 6.74 1.43 36 4 -2 6.27 1.36 38 4 -2 23.73 2.17 38 4 -2 26.75 2.23 40 4 -2 40.60 2.56 42 4 -2 74.87 3.11 44 4 -2 41.85 2.43 46 4 -2 2.92 0.97 48 4 -2 53.12 2.37 -46 4 -3 72.45 2.90 46 -4 3 64.15 2.81 -44 4 -3 30.34 2.29 44 -4 3 28.47 2.22 44 -4 3 32.60 1.99 -42 4 -3 3.84 1.23 42 -4 3 1.87 1.09 42 -4 3 3.73 1.19 -40 4 -3 30.35 2.52 40 -4 3 26.66 2.48 40 -4 3 32.47 2.40 -38 4 -3 0.09 0.99 38 -4 3 1.71 1.16 -36 4 -3 27.58 2.56 36 -4 3 29.02 2.48 -34 4 -3 13.49 2.18 -34 4 -3 10.26 2.07 34 -4 3 13.64 2.04 -32 4 -3 75.64 3.68 -32 4 -3 64.56 3.46 32 -4 3 86.98 3.88 -30 4 -3 0.99 0.85 -30 4 -3 1.16 1.26 30 -4 3 -0.32 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22 -4 4 76.02 3.30 -20 4 -4 8.59 1.39 -20 4 -4 10.17 1.53 20 -4 4 9.86 1.61 -18 4 -4 506.72 7.24 -18 4 -4 551.82 6.81 18 -4 4 514.34 7.42 -16 4 -4 39.65 2.18 -16 4 -4 36.64 2.14 -16 4 -4 40.80 2.02 16 -4 4 31.63 2.16 -14 4 -4 437.88 5.45 -12 4 -4 135.65 2.95 -10 4 -4 5.48 0.89 -8 4 -4 1.42 0.60 -6 4 -4 651.43 4.97 6 4 -4 147.70 3.59 8 4 -4 136.56 3.59 -8 -4 4 155.20 3.70 10 4 -4 407.64 6.10 -10 -4 4 479.19 6.54 12 4 -4 167.51 4.21 12 4 -4 158.95 3.99 14 4 -4 134.50 2.81 14 4 -4 153.56 4.14 14 4 -4 135.92 3.81 16 4 -4 133.40 3.96 16 4 -4 118.93 3.69 18 4 -4 18.82 2.33 18 4 -4 17.10 2.00 18 4 -4 14.61 1.85 20 4 -4 19.29 1.65 20 4 -4 25.94 2.33 20 4 -4 28.46 2.33 20 4 -4 23.49 2.20 22 4 -4 958.16 10.87 22 4 -4 1141.23 11.55 22 4 -4 817.77 9.75 24 4 -4 24.79 1.94 24 4 -4 27.32 2.39 26 4 -4 9.32 1.41 26 4 -4 8.24 1.86 28 4 -4 4.40 1.14 30 4 -4 5.22 1.28 32 4 -4 43.37 2.58 32 4 -4 49.20 2.76 34 4 -4 201.23 4.93 34 4 -4 230.66 5.20 36 4 -4 0.29 0.91 36 4 -4 -0.42 0.84 38 4 -4 1.29 1.06 38 4 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2.98 -10 4 -5 85.00 2.43 -8 4 -5 3.09 0.77 -6 4 -5 34.04 1.49 8 4 -5 123.10 2.92 8 4 -5 116.72 3.55 10 4 -5 12.57 1.27 10 4 -5 11.87 1.67 12 4 -5 17.09 1.37 12 4 -5 15.49 1.86 -12 -4 5 16.90 1.65 14 4 -5 12.32 1.27 14 4 -5 14.66 1.96 14 4 -5 12.09 1.76 -14 -4 5 13.42 1.55 16 4 -5 4.37 1.32 16 4 -5 4.30 1.34 -16 -4 5 4.76 1.31 18 4 -5 66.58 3.20 18 4 -5 75.92 3.41 18 4 -5 57.49 2.96 -18 -4 5 63.86 3.00 20 4 -5 214.40 5.40 20 4 -5 247.83 5.78 20 4 -5 176.61 4.84 -20 -4 5 197.19 5.18 22 4 -5 16.88 2.22 22 4 -5 19.37 2.46 22 4 -5 12.84 2.08 -22 -4 5 13.72 1.99 24 4 -5 39.67 2.89 24 4 -5 53.60 3.22 24 4 -5 36.15 2.74 -24 -4 5 35.62 2.61 26 4 -5 1.81 0.98 26 4 -5 4.00 1.61 -26 -4 5 2.35 1.25 28 4 -5 24.31 2.15 28 4 -5 23.36 2.60 30 4 -5 26.52 2.34 32 4 -5 1.83 1.14 34 4 -5 0.40 0.98 34 4 -5 0.63 0.99 36 4 -5 1.78 1.08 36 4 -5 2.99 1.12 38 4 -5 1.41 1.02 38 4 -5 -0.37 0.93 40 4 -5 39.26 2.45 40 4 -5 47.56 2.53 42 4 -5 6.39 1.26 42 4 -5 6.79 1.27 44 4 -5 13.04 1.53 -42 4 -6 0.97 0.75 -40 4 -6 79.62 3.17 -38 4 -6 1.34 0.98 -36 4 -6 13.12 1.92 -34 4 -6 105.01 4.07 34 -4 6 114.90 4.06 -32 4 -6 29.42 2.51 32 -4 6 29.13 2.37 32 -4 6 30.65 2.55 -30 4 -6 40.42 2.83 30 -4 6 42.84 2.79 30 -4 6 46.55 3.04 -28 4 -6 38.20 2.76 -28 4 -6 37.52 2.75 28 -4 6 43.80 2.98 -26 4 -6 60.85 3.28 -26 4 -6 62.76 3.16 26 -4 6 69.50 3.53 -24 4 -6 6.78 1.56 -24 4 -6 5.86 1.54 24 -4 6 6.04 1.55 -22 4 -6 6.50 1.49 -22 4 -6 5.26 1.36 22 -4 6 6.42 1.49 -20 4 -6 19.34 1.94 -20 4 -6 22.48 2.03 20 -4 6 18.62 2.14 -18 4 -6 202.12 5.11 -18 4 -6 203.84 4.63 18 -4 6 183.68 4.97 -16 4 -6 37.75 2.38 -16 4 -6 34.92 2.12 16 -4 6 35.61 2.46 -14 4 -6 466.98 7.21 -14 4 -6 419.57 6.95 -14 4 -6 464.05 6.32 14 -4 6 452.36 7.28 -12 4 -6 238.34 5.05 -12 4 -6 229.28 5.06 -12 4 -6 228.01 4.31 12 -4 6 236.94 5.25 -10 4 -6 64.79 2.70 -10 4 -6 63.39 2.77 -10 4 -6 56.87 2.24 10 -4 6 60.65 2.86 -8 4 -6 33.61 2.02 -8 4 -6 39.12 2.24 -8 4 -6 33.22 1.74 8 -4 6 35.23 2.34 -6 4 -6 6.25 1.14 -6 4 -6 6.23 1.18 -6 4 -6 5.06 0.92 -4 4 -6 132.23 3.39 -4 4 -6 157.42 3.84 -4 4 -6 115.99 2.57 -4 4 -6 153.44 4.01 -2 4 -6 182.27 3.85 -2 4 -6 208.22 4.29 -2 4 -6 220.56 5.07 -2 4 -6 209.02 4.62 0 4 -6 44.58 2.18 0 4 -6 46.87 2.56 0 4 -6 47.50 2.53 2 4 -6 29.79 1.85 2 4 -6 27.52 2.14 4 4 -6 106.11 3.06 4 4 -6 120.24 3.89 6 4 -6 6.10 1.11 6 4 -6 4.87 1.25 8 4 -6 386.66 5.06 8 4 -6 431.63 5.91 8 4 -6 452.48 7.31 10 4 -6 36.18 1.77 10 4 -6 38.42 2.05 10 4 -6 43.21 2.70 10 4 -6 34.30 2.42 12 4 -6 6.76 1.05 12 4 -6 6.68 1.17 12 4 -6 10.09 1.78 12 4 -6 8.14 1.61 14 4 -6 335.01 4.63 14 4 -6 388.80 7.08 14 4 -6 323.00 6.49 16 4 -6 0.58 0.67 16 4 -6 0.63 1.08 16 4 -6 1.31 1.19 18 4 -6 29.65 1.64 18 4 -6 37.77 2.77 18 4 -6 28.61 2.53 -18 -4 6 33.08 2.47 20 4 -6 342.35 4.60 20 4 -6 455.13 7.97 20 4 -6 504.36 8.47 20 4 -6 327.90 6.81 -20 -4 6 401.65 7.63 22 4 -6 20.80 2.57 22 4 -6 23.10 2.83 -22 -4 6 16.85 2.05 24 4 -6 156.24 4.95 24 4 -6 198.57 5.67 26 4 -6 335.69 6.99 26 4 -6 368.77 6.50 26 4 -6 425.15 7.99 28 4 -6 2.07 1.06 28 4 -6 3.47 1.67 30 4 -6 126.59 4.05 30 4 -6 141.83 4.78 32 4 -6 1.51 1.03 34 4 -6 12.01 1.77 34 4 -6 11.04 1.69 36 4 -6 112.43 3.78 36 4 -6 123.34 3.86 38 4 -6 81.03 3.22 38 4 -6 88.46 3.21 40 4 -6 0.07 0.90 40 4 -6 0.49 0.89 42 4 -6 13.94 1.67 42 4 -6 15.18 1.58 -40 4 -7 19.83 1.71 -38 4 -7 1.02 0.82 -36 4 -7 0.75 0.84 -34 4 -7 4.50 1.20 -32 4 -7 66.68 3.30 32 -4 7 67.79 3.18 -30 4 -7 -0.29 0.79 30 -4 7 1.48 1.08 -28 4 -7 52.95 3.09 28 -4 7 59.29 3.22 -26 4 -7 43.31 2.87 26 -4 7 47.72 3.03 -24 4 -7 6.70 1.49 -24 4 -7 5.86 1.56 24 -4 7 7.88 1.80 24 -4 7 7.19 1.65 -22 4 -7 1.77 0.99 -22 4 -7 2.08 1.15 22 -4 7 1.56 1.19 -20 4 -7 36.26 2.55 -20 4 -7 37.51 2.48 20 -4 7 40.01 2.83 -18 4 -7 35.61 2.47 -18 4 -7 33.71 2.33 18 -4 7 32.76 2.62 -16 4 -7 22.18 2.08 -16 4 -7 24.29 2.01 16 -4 7 19.74 2.21 -14 4 -7 21.56 1.95 -14 4 -7 22.89 1.92 14 -4 7 17.92 2.13 -12 4 -7 34.25 2.26 -12 4 -7 31.01 2.35 -12 4 -7 31.12 2.02 -10 4 -7 29.65 2.12 -10 4 -7 31.07 2.25 -10 4 -7 27.89 1.87 -10 4 -7 30.87 2.22 -8 4 -7 91.09 3.27 -8 4 -7 89.94 3.38 -8 4 -7 79.29 2.63 -6 4 -7 248.31 5.06 -6 4 -7 264.48 5.44 -6 4 -7 213.50 3.89 -4 4 -7 4.80 1.10 -4 4 -7 4.92 1.17 -4 4 -7 4.14 0.88 -2 4 -7 117.26 3.42 -2 4 -7 123.02 3.72 -2 4 -7 134.76 4.35 -2 4 -7 131.05 3.96 0 4 -7 77.25 2.80 0 4 -7 83.36 3.09 0 4 -7 93.41 3.69 0 4 -7 88.88 3.46 0 -4 7 80.68 3.34 2 4 -7 0.22 0.68 2 4 -7 0.41 0.75 2 4 -7 0.90 0.99 -2 -4 7 0.33 0.87 4 4 -7 2.91 0.91 4 4 -7 1.05 0.87 4 4 -7 2.72 1.23 6 4 -7 32.01 1.91 6 4 -7 33.12 2.13 6 4 -7 37.00 2.61 8 4 -7 36.28 2.00 8 4 -7 36.02 2.22 8 4 -7 39.27 2.71 10 4 -7 14.83 1.51 10 4 -7 17.41 1.75 10 4 -7 16.69 2.07 10 4 -7 14.34 2.05 12 4 -7 14.14 1.47 12 4 -7 12.36 1.61 12 4 -7 16.64 2.23 12 4 -7 11.24 1.94 14 4 -7 174.92 3.72 14 4 -7 207.74 5.56 14 4 -7 155.59 4.93 16 4 -7 46.04 2.13 16 4 -7 55.01 3.23 18 4 -7 11.22 1.33 18 4 -7 15.00 2.28 20 4 -7 82.98 2.60 20 4 -7 107.17 4.26 20 4 -7 117.41 4.59 22 4 -7 1.01 0.76 22 4 -7 1.21 1.38 22 4 -7 1.71 1.48 24 4 -7 -0.56 1.20 24 4 -7 0.84 1.40 26 4 -7 19.02 2.49 26 4 -7 27.41 2.85 28 4 -7 37.98 2.62 28 4 -7 46.40 3.26 30 4 -7 5.08 1.34 30 4 -7 7.77 1.97 32 4 -7 46.76 2.75 32 4 -7 50.79 3.20 34 4 -7 19.31 2.11 36 4 -7 56.91 2.81 36 4 -7 65.10 2.88 38 4 -7 2.25 1.10 38 4 -7 2.85 1.04 40 4 -7 1.94 1.00 40 4 -7 1.60 0.89 -38 4 -8 11.54 1.44 -36 4 -8 118.35 3.52 -34 4 -8 25.81 2.06 -32 4 -8 4.03 1.23 32 -4 8 4.44 1.26 -30 4 -8 25.74 2.21 30 -4 8 28.97 2.35 -28 4 -8 79.27 3.51 28 -4 8 83.88 3.62 -26 4 -8 74.51 3.45 26 -4 8 88.84 3.85 -24 4 -8 84.27 3.69 24 -4 8 94.02 4.00 -22 4 -8 130.22 4.49 22 -4 8 145.01 4.95 -20 4 -8 33.94 2.51 -20 4 -8 33.12 2.35 20 -4 8 37.92 2.86 -18 4 -8 58.85 3.13 -18 4 -8 53.11 2.69 18 -4 8 57.16 3.34 -16 4 -8 14.74 2.04 -16 4 -8 14.15 1.76 16 -4 8 16.05 2.35 -14 4 -8 121.41 4.14 -14 4 -8 116.52 3.57 14 -4 8 116.08 4.46 -12 4 -8 376.24 6.97 -12 4 -8 335.80 5.63 12 -4 8 296.09 6.83 -10 4 -8 434.23 7.35 -10 4 -8 412.04 7.48 -10 4 -8 389.59 5.85 10 -4 8 379.71 7.61 -8 4 -8 48.06 2.66 -8 4 -8 43.15 2.79 -8 4 -8 40.01 2.19 8 -4 8 46.45 2.97 -6 4 -8 30.76 2.21 -6 4 -8 29.37 2.32 -6 4 -8 24.09 1.78 6 -4 8 30.06 2.55 -4 4 -8 18.26 1.82 -4 4 -8 19.87 2.05 -4 4 -8 15.07 1.51 -4 4 -8 25.91 2.51 4 -4 8 20.89 2.27 -2 4 -8 185.26 4.55 -2 4 -8 193.06 4.96 -2 4 -8 238.33 6.02 -2 4 -8 207.09 5.12 2 -4 8 208.55 5.45 0 4 -8 571.36 7.69 0 4 -8 584.47 8.34 0 4 -8 659.78 9.80 0 4 -8 637.16 8.96 0 -4 8 588.10 8.79 2 4 -8 26.81 2.19 2 4 -8 26.28 2.59 2 4 -8 25.38 2.41 -2 -4 8 23.27 2.21 4 4 -8 6.20 1.22 4 4 -8 6.07 1.37 4 4 -8 7.51 1.70 -4 -4 8 7.06 1.70 6 4 -8 15.22 1.62 6 4 -8 13.85 1.82 6 4 -8 16.03 2.21 8 4 -8 10.22 1.48 8 4 -8 9.73 1.59 8 4 -8 12.33 2.17 10 4 -8 31.88 2.02 10 4 -8 30.83 2.26 10 4 -8 32.05 2.73 12 4 -8 460.14 6.35 12 4 -8 503.95 8.67 14 4 -8 6.03 1.17 14 4 -8 5.36 1.77 16 4 -8 0.35 0.77 16 4 -8 0.12 1.29 18 4 -8 13.51 1.50 18 4 -8 20.28 2.67 18 4 -8 21.79 2.64 20 4 -8 23.07 1.66 20 4 -8 27.99 2.81 20 4 -8 36.17 3.12 22 4 -8 212.42 5.72 22 4 -8 249.54 6.54 24 4 -8 95.42 4.01 24 4 -8 134.28 4.98 26 4 -8 22.88 2.49 26 4 -8 25.52 2.87 28 4 -8 2.90 1.17 28 4 -8 1.94 1.60 30 4 -8 16.69 2.09 30 4 -8 17.67 2.54 32 4 -8 22.30 2.13 32 4 -8 25.57 2.62 34 4 -8 137.72 3.99 34 4 -8 151.45 4.03 36 4 -8 94.00 3.23 36 4 -8 101.41 3.17 38 4 -8 18.01 1.79 38 4 -8 24.51 1.78 -34 4 -9 23.43 1.74 -32 4 -9 24.08 1.84 32 -4 9 20.47 1.82 -30 4 -9 0.04 0.71 30 -4 9 0.41 0.92 -28 4 -9 7.62 1.47 -28 4 -9 7.92 1.56 28 -4 9 9.33 1.67 -26 4 -9 0.06 0.73 26 -4 9 0.76 1.07 -24 4 -9 38.73 2.53 24 -4 9 44.05 2.91 -22 4 -9 2.56 1.01 22 -4 9 4.47 1.45 -20 4 -9 130.02 4.38 20 -4 9 139.35 4.83 -18 4 -9 49.28 2.83 18 -4 9 49.42 3.17 -16 4 -9 13.24 1.95 16 -4 9 9.61 1.82 -14 4 -9 20.37 2.04 -14 4 -9 18.87 1.82 14 -4 9 15.60 2.21 -12 4 -9 11.21 1.74 -12 4 -9 10.63 1.56 12 -4 9 8.55 1.89 -10 4 -9 10.15 1.71 -10 4 -9 9.99 1.39 10 -4 9 9.90 1.85 -8 4 -9 7.96 1.52 -8 4 -9 6.54 1.21 -8 4 -9 10.31 2.05 8 -4 9 7.08 1.65 -6 4 -9 6.91 1.48 -6 4 -9 7.65 1.71 -6 4 -9 9.35 1.94 6 -4 9 6.38 1.62 -4 4 -9 25.66 2.15 -4 4 -9 25.02 2.36 -4 4 -9 30.95 2.76 4 -4 9 24.84 2.43 -2 4 -9 8.32 1.54 -2 4 -9 6.99 1.53 -2 4 -9 9.56 1.98 2 -4 9 9.38 1.82 0 4 -9 32.75 2.29 0 4 -9 32.18 2.53 0 4 -9 42.21 3.12 0 4 -9 40.31 2.76 0 -4 9 38.83 2.83 2 4 -9 189.55 4.68 2 4 -9 181.41 5.04 2 4 -9 217.74 6.03 2 4 -9 198.25 5.43 -2 -4 9 177.16 5.10 4 4 -9 7.12 1.38 4 4 -9 5.93 1.43 4 4 -9 8.14 1.93 4 4 -9 8.80 1.85 6 4 -9 31.92 2.20 6 4 -9 29.76 2.42 6 4 -9 32.11 2.80 6 4 -9 32.63 2.81 8 4 -9 16.48 1.77 8 4 -9 12.95 1.83 8 4 -9 15.16 2.31 10 4 -9 1.77 0.94 10 4 -9 0.11 1.29 12 4 -9 -0.48 0.75 12 4 -9 1.32 1.34 14 4 -9 6.85 1.27 14 4 -9 8.10 1.96 14 4 -9 8.06 1.95 16 4 -9 0.57 0.84 16 4 -9 0.17 1.27 16 4 -9 1.12 1.35 18 4 -9 13.71 1.49 18 4 -9 18.44 2.44 18 4 -9 17.63 2.61 20 4 -9 8.46 1.16 20 4 -9 10.38 2.12 20 4 -9 12.22 2.36 22 4 -9 12.70 2.13 22 4 -9 18.07 2.74 24 4 -9 11.54 2.00 24 4 -9 14.70 2.40 26 4 -9 14.46 1.89 26 4 -9 20.40 2.72 28 4 -9 31.08 2.40 28 4 -9 39.77 2.99 30 4 -9 2.45 1.12 30 4 -9 3.15 1.57 32 4 -9 -0.48 0.81 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2.58 1.54 13 5 -8 4.06 1.67 13 5 -8 3.50 1.61 15 5 -8 163.96 5.35 15 5 -8 167.72 5.48 17 5 -8 2.13 1.43 17 5 -8 0.06 1.36 19 5 -8 374.70 7.70 19 5 -8 417.68 8.35 21 5 -8 0.48 1.35 21 5 -8 1.28 1.46 23 5 -8 0.19 1.32 23 5 -8 0.31 1.46 25 5 -8 57.30 3.26 25 5 -8 57.00 2.75 25 5 -8 68.42 3.78 27 5 -8 27.19 2.12 27 5 -8 29.68 2.85 29 5 -8 22.62 1.97 29 5 -8 26.61 2.61 31 5 -8 70.27 2.68 31 5 -8 76.19 3.49 33 5 -8 1.35 0.91 33 5 -8 0.91 0.82 33 5 -8 0.10 1.29 35 5 -8 1.06 0.87 35 5 -8 0.69 0.71 37 5 -8 121.55 3.03 37 5 -8 133.79 2.49 -33 5 -9 70.92 2.27 -31 5 -9 2.17 0.79 31 -5 9 2.39 0.97 -29 5 -9 5.63 1.11 29 -5 9 7.21 1.41 -27 5 -9 73.89 2.84 27 -5 9 83.25 3.32 -25 5 -9 0.29 0.74 25 -5 9 0.35 1.00 -23 5 -9 11.61 1.65 -23 5 -9 15.15 2.07 23 -5 9 12.09 1.98 -21 5 -9 22.66 1.97 -21 5 -9 22.11 2.22 21 -5 9 22.18 2.32 -19 5 -9 2.70 1.02 -19 5 -9 2.39 1.32 19 -5 9 1.77 1.15 -17 5 -9 25.71 2.10 -17 5 -9 32.81 2.62 17 -5 9 26.95 2.51 -15 5 -9 74.57 3.16 -15 5 -9 76.70 3.67 15 -5 9 67.63 3.56 -13 5 -9 60.84 2.89 -13 5 -9 65.13 3.50 13 -5 9 49.91 3.16 -11 5 -9 3.33 1.08 -11 5 -9 3.90 1.33 -11 5 -9 3.93 1.47 11 -5 9 2.57 1.33 -9 5 -9 28.70 2.12 -9 5 -9 26.22 2.42 -9 5 -9 30.62 2.75 9 -5 9 24.56 2.46 -7 5 -9 4.34 1.14 -7 5 -9 2.57 1.24 -7 5 -9 4.93 1.70 7 -5 9 3.76 1.43 -5 5 -9 57.01 2.66 -5 5 -9 58.85 3.17 -5 5 -9 67.86 3.69 5 -5 9 57.57 3.28 -3 5 -9 4.73 1.13 -3 5 -9 5.41 1.41 -3 5 -9 5.72 1.76 3 -5 9 6.34 1.60 -1 5 -9 11.29 1.47 -1 5 -9 11.09 1.81 -1 5 -9 12.55 2.21 -1 5 -9 13.87 2.21 1 -5 9 11.68 1.98 1 5 -9 48.57 2.34 1 5 -9 47.22 2.85 1 5 -9 56.94 3.46 1 5 -9 51.33 3.17 -1 -5 9 47.87 2.99 3 5 -9 3.99 1.02 3 5 -9 2.91 1.20 3 5 -9 3.57 1.46 3 5 -9 4.49 1.58 5 5 -9 24.76 1.79 5 5 -9 25.69 2.28 5 5 -9 34.71 2.96 5 5 -9 29.41 2.71 7 5 -9 246.30 4.20 7 5 -9 248.33 5.67 7 5 -9 286.65 6.95 7 5 -9 271.34 6.60 9 5 -9 55.79 3.48 9 5 -9 50.86 3.36 11 5 -9 30.20 2.86 11 5 -9 27.37 2.86 13 5 -9 0.10 1.31 13 5 -9 0.44 1.40 15 5 -9 23.76 2.64 15 5 -9 23.21 2.78 17 5 -9 22.48 2.59 17 5 -9 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2.97 -5 5 -10 58.12 3.47 5 -5 10 51.37 3.08 -3 5 -10 86.45 3.01 -3 5 -10 80.16 3.58 -3 5 -10 100.60 4.30 3 -5 10 83.27 3.68 -1 5 -10 23.56 1.85 -1 5 -10 22.61 2.24 -1 5 -10 34.74 2.87 1 -5 10 25.04 2.38 1 5 -10 115.43 3.23 1 5 -10 112.46 4.07 1 5 -10 130.05 4.79 1 5 -10 116.49 4.24 -1 -5 10 106.22 4.01 3 5 -10 3.75 0.99 3 5 -10 2.25 1.17 3 5 -10 4.88 1.63 3 5 -10 3.24 1.51 5 5 -10 17.24 1.53 5 5 -10 22.88 2.20 5 5 -10 25.79 2.71 5 5 -10 24.76 2.68 7 5 -10 179.76 5.52 7 5 -10 172.72 5.30 9 5 -10 12.03 2.14 9 5 -10 11.64 2.29 11 5 -10 80.71 3.86 11 5 -10 82.02 3.95 13 5 -10 22.03 2.50 13 5 -10 22.66 2.65 15 5 -10 64.82 3.41 15 5 -10 71.64 3.73 17 5 -10 3.69 1.54 17 5 -10 2.82 1.54 19 5 -10 98.78 3.86 19 5 -10 112.72 4.38 21 5 -10 -0.03 1.13 21 5 -10 1.00 1.38 23 5 -10 88.47 3.04 23 5 -10 106.89 4.05 25 5 -10 7.36 1.28 25 5 -10 10.15 1.91 27 5 -10 46.02 2.11 27 5 -10 50.43 2.81 29 5 -10 21.68 1.54 -21 5 -11 5.25 0.91 -21 5 -11 6.46 1.27 21 -5 11 6.23 1.27 -19 5 -11 70.24 2.28 -19 5 -11 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1.72 -4 6 6 409.27 6.77 -4 6 6 415.91 7.82 -2 6 6 192.31 4.66 -2 6 6 198.39 5.47 0 6 6 61.77 2.81 0 6 6 43.36 2.45 0 6 6 61.86 3.28 2 6 6 48.78 2.52 2 6 6 34.84 2.24 2 6 6 43.54 2.85 4 6 6 0.63 0.71 4 6 6 -0.31 0.66 4 6 6 0.90 0.97 6 6 6 33.94 2.17 6 6 6 25.12 1.98 6 6 6 30.14 2.46 8 6 6 369.81 6.21 8 6 6 287.42 5.62 8 6 6 318.85 6.60 10 6 6 222.92 4.90 10 6 6 167.74 4.37 10 6 6 193.38 5.16 12 6 6 40.71 2.36 12 6 6 36.21 2.57 14 6 6 31.50 2.17 16 6 6 6.37 1.30 18 6 6 167.95 4.40 20 6 6 31.79 2.22 22 6 6 30.64 2.17 24 6 6 3.41 1.09 26 6 6 5.11 1.22 28 6 6 54.42 2.68 30 6 6 203.65 4.65 -30 -6 -6 216.62 5.43 32 6 6 8.30 1.33 -32 -6 -6 9.58 1.73 34 6 6 17.16 1.68 -34 -6 -6 16.32 1.83 36 6 6 22.08 1.73 -36 -6 -6 21.22 1.82 38 6 6 33.75 1.91 -42 6 5 -0.22 0.69 -40 6 5 39.26 2.19 40 -6 -5 38.63 2.16 -38 6 5 34.04 2.24 38 -6 -5 34.57 2.33 -36 6 5 44.28 2.62 36 -6 -5 43.29 2.70 -34 6 5 13.32 1.87 34 -6 -5 15.02 2.10 -32 6 5 0.47 1.04 32 -6 -5 0.04 1.18 -30 6 5 27.83 2.43 30 -6 -5 24.90 2.65 -28 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326.03 4.31 2 6 3 367.96 6.27 2 6 3 350.10 6.06 2 6 3 310.70 3.31 4 6 3 179.41 3.20 4 6 3 162.75 3.02 4 6 3 169.05 4.29 4 6 3 176.31 4.40 4 6 3 156.40 2.26 6 6 3 120.74 2.64 6 6 3 109.04 2.46 6 6 3 121.74 3.75 6 6 3 105.94 1.83 8 6 3 41.46 1.66 8 6 3 40.37 1.60 8 6 3 45.52 2.52 8 6 3 35.83 1.11 10 6 3 17.74 1.21 10 6 3 16.02 1.14 10 6 3 21.55 1.97 12 6 3 244.14 3.77 12 6 3 243.87 3.70 12 6 3 265.59 5.71 12 6 3 305.75 6.07 14 6 3 48.97 1.88 14 6 3 48.27 1.82 14 6 3 50.78 2.79 14 6 3 60.72 3.01 16 6 3 189.68 3.55 16 6 3 184.58 3.42 16 6 3 210.81 5.34 16 6 3 228.82 5.43 -16 -6 -3 247.40 5.89 18 6 3 39.20 1.86 18 6 3 35.06 1.76 18 6 3 49.17 2.84 -18 -6 -3 50.94 3.04 20 6 3 0.93 0.65 20 6 3 0.61 0.59 20 6 3 1.43 1.09 22 6 3 17.27 1.52 22 6 3 11.19 1.33 22 6 3 20.18 2.24 24 6 3 144.28 3.59 24 6 3 174.95 5.06 26 6 3 16.41 1.61 28 6 3 24.56 1.88 30 6 3 2.88 0.95 32 6 3 5.43 1.17 34 6 3 15.13 1.66 36 6 3 47.75 2.36 38 6 3 91.47 2.94 40 6 3 2.65 0.87 42 6 3 0.64 0.63 -44 6 2 16.15 1.59 44 -6 -2 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259.99 5.34 10 6 1 252.64 5.37 12 6 1 11.77 1.69 12 6 1 11.10 1.76 14 6 1 17.86 0.95 14 6 1 21.20 2.02 14 6 1 23.47 2.11 -14 -6 -1 25.19 2.06 16 6 1 17.27 1.01 16 6 1 19.33 1.98 16 6 1 22.04 2.07 -16 -6 -1 21.05 2.00 18 6 1 2.81 0.63 18 6 1 2.13 0.53 18 6 1 1.90 1.06 18 6 1 3.08 1.28 20 6 1 262.89 3.73 20 6 1 258.20 3.42 20 6 1 379.50 7.17 22 6 1 58.19 2.01 22 6 1 93.21 3.85 24 6 1 1.00 0.64 24 6 1 0.47 0.98 26 6 1 19.83 1.54 28 6 1 6.23 1.13 30 6 1 14.44 1.54 32 6 1 62.28 2.56 34 6 1 10.41 1.43 36 6 1 3.95 1.03 38 6 1 28.22 1.91 40 6 1 1.06 0.77 42 6 1 20.67 1.54 44 6 1 26.30 1.49 -44 6 0 13.24 1.50 44 -6 0 13.83 1.57 -42 6 0 71.84 2.92 42 -6 0 80.14 3.07 -40 6 0 52.52 2.72 40 -6 0 58.77 2.93 -38 6 0 47.29 2.74 38 -6 0 53.92 3.05 -36 6 0 4.51 1.31 36 -6 0 3.82 1.45 -34 6 0 23.18 2.21 34 -6 0 26.53 2.60 -32 6 0 11.34 1.75 32 -6 0 12.75 2.13 -30 6 0 4.82 1.34 -30 6 0 4.52 1.26 30 -6 0 5.47 1.61 -28 6 0 20.03 2.08 -28 6 0 13.64 1.65 28 -6 0 22.53 2.61 -26 6 0 66.44 3.11 -26 6 0 62.02 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71.36 2.52 24 6 -6 77.76 3.98 26 6 -6 35.72 1.93 26 6 -6 35.92 3.06 28 6 -6 2.30 0.89 28 6 -6 5.19 1.79 30 6 -6 61.02 2.16 30 6 -6 56.71 3.33 32 6 -6 49.19 2.31 32 6 -6 50.13 1.86 34 6 -6 4.22 1.02 34 6 -6 5.07 0.78 36 6 -6 10.95 1.30 38 6 -6 0.04 0.65 -36 6 -7 4.60 0.82 -34 6 -7 50.36 2.11 34 -6 7 43.02 2.25 -32 6 -7 -0.17 0.62 32 -6 7 0.34 0.84 -30 6 -7 0.03 0.71 30 -6 7 0.34 0.98 -28 6 -7 62.85 2.71 28 -6 7 70.48 3.33 -26 6 -7 84.55 3.15 26 -6 7 94.90 3.89 -24 6 -7 0.31 0.80 -22 6 -7 16.23 1.70 22 -6 7 17.28 2.30 -20 6 -7 1.68 0.87 -20 6 -7 1.16 1.10 20 -6 7 1.24 1.14 -18 6 -7 33.30 2.13 -18 6 -7 32.54 2.49 18 -6 7 32.28 2.65 -16 6 -7 3.75 1.05 -16 6 -7 4.61 1.34 -16 6 -7 2.76 1.35 16 -6 7 4.66 1.40 -14 6 -7 1.17 0.76 -14 6 -7 1.13 0.97 -14 6 -7 1.08 1.18 -12 6 -7 184.57 4.21 -12 6 -7 196.26 5.14 -12 6 -7 189.17 5.31 -10 6 -7 2.21 0.85 -10 6 -7 1.98 0.98 -10 6 -7 2.53 1.28 -8 6 -7 0.45 0.68 -8 6 -7 0.25 0.79 -8 6 -7 0.80 1.17 -6 6 -7 58.32 2.24 -6 6 -7 71.84 3.13 -6 6 -7 72.45 3.56 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2.52 -21 7 7 9.16 1.46 21 -7 -7 11.29 2.06 -19 7 7 3.03 1.08 19 -7 -7 0.43 1.28 -17 7 7 10.17 1.54 -17 7 7 10.54 1.85 17 -7 -7 12.27 2.15 -15 7 7 0.93 0.92 -15 7 7 0.51 1.07 15 -7 -7 1.57 1.39 -13 7 7 477.73 6.83 -13 7 7 569.25 8.83 -11 7 7 34.90 2.21 -11 7 7 45.68 2.99 -9 7 7 2.44 0.94 -9 7 7 2.21 1.30 -7 7 7 48.69 2.30 -7 7 7 70.64 3.39 -7 7 7 69.85 3.80 -5 7 7 13.73 1.53 -5 7 7 18.19 2.24 -5 7 7 18.28 2.47 -3 7 7 116.25 2.99 -3 7 7 175.20 4.87 -3 7 7 167.08 5.40 -1 7 7 230.01 5.42 -1 7 7 227.84 6.21 1 7 7 14.01 1.93 1 7 7 10.41 1.92 3 7 7 41.90 2.57 3 7 7 42.77 3.07 5 7 7 161.86 4.47 5 7 7 142.25 4.86 7 7 7 7.88 1.51 7 7 7 8.18 1.76 9 7 7 134.47 4.04 9 7 7 124.01 4.40 11 7 7 72.39 3.06 11 7 7 66.86 3.33 13 7 7 83.08 3.22 15 7 7 66.33 2.91 17 7 7 19.74 1.90 19 7 7 -0.03 0.80 21 7 7 35.23 2.20 23 7 7 213.25 4.57 25 7 7 49.64 2.36 27 7 7 84.47 2.81 29 7 7 2.46 0.87 31 7 7 31.83 1.72 -37 7 6 -0.44 0.58 -35 7 6 24.37 1.66 35 -7 -6 23.65 1.94 -33 7 6 7.20 1.22 33 -7 -6 9.95 1.63 -31 7 6 35.77 2.15 31 -7 -6 34.72 2.59 -29 7 6 27.12 2.06 29 -7 -6 25.32 2.48 -27 7 6 16.79 1.90 27 -7 -6 14.67 2.13 -25 7 6 29.88 2.23 25 -7 -6 21.89 2.48 -23 7 6 9.32 1.54 23 -7 -6 8.26 1.84 -21 7 6 7.35 1.41 -21 7 6 6.14 1.74 21 -7 -6 9.31 1.97 -19 7 6 9.28 1.48 -19 7 6 8.42 1.68 19 -7 -6 10.59 2.13 -17 7 6 0.93 0.95 -17 7 6 0.28 1.13 17 -7 -6 1.78 1.43 -15 7 6 5.13 1.19 -15 7 6 4.16 1.37 15 -7 -6 6.18 1.81 -13 7 6 14.51 1.71 -13 7 6 18.07 2.22 -11 7 6 5.28 1.16 -11 7 6 6.24 1.60 -9 7 6 319.60 5.25 -9 7 6 428.76 7.39 -7 7 6 25.44 1.81 -7 7 6 39.69 2.68 -7 7 6 37.32 3.10 -5 7 6 12.27 1.47 -5 7 6 20.20 2.10 -5 7 6 17.47 2.38 -3 7 6 58.04 2.92 -3 7 6 56.62 3.44 -1 7 6 0.46 0.87 -1 7 6 0.35 1.08 1 7 6 25.28 2.07 1 7 6 22.13 2.51 3 7 6 90.39 3.31 3 7 6 82.72 3.82 5 7 6 76.86 3.09 5 7 6 65.89 3.43 7 7 6 3.73 1.08 7 7 6 4.63 1.42 9 7 6 72.06 2.96 9 7 6 65.69 3.34 9 7 6 72.64 3.40 11 7 6 26.12 2.02 11 7 6 21.52 2.31 11 7 6 25.48 2.35 13 7 6 53.50 2.62 15 7 6 1.52 0.93 17 7 6 1.33 0.88 19 7 6 10.17 1.53 21 7 6 2.04 0.95 23 7 6 16.62 1.75 25 7 6 55.34 2.54 27 7 6 14.38 1.62 29 7 6 0.29 0.73 31 7 6 26.64 1.75 -31 -7 -6 22.07 1.96 33 7 6 28.34 1.67 -39 7 5 24.65 1.57 -37 7 5 4.75 0.97 37 -7 -5 4.28 1.21 -35 7 5 13.15 1.56 35 -7 -5 15.13 1.89 -33 7 5 62.34 2.69 33 -7 -5 67.14 3.18 -31 7 5 132.65 3.87 31 -7 -5 132.96 4.37 -29 7 5 3.17 1.10 29 -7 -5 3.14 1.49 -27 7 5 0.94 0.99 27 -7 -5 0.27 1.26 -25 7 5 5.97 1.39 25 -7 -5 3.65 1.53 -23 7 5 -0.29 0.81 -23 7 5 0.09 1.18 23 -7 -5 1.60 1.40 -21 7 5 199.93 4.81 -21 7 5 193.26 5.41 21 -7 -5 199.94 5.59 -19 7 5 1.36 0.98 -19 7 5 1.69 1.27 19 -7 -5 3.11 1.55 -17 7 5 16.84 1.77 -17 7 5 15.24 2.04 17 -7 -5 19.15 2.45 -15 7 5 1.54 0.88 -15 7 5 1.52 1.09 -13 7 5 24.63 1.91 -13 7 5 28.90 2.40 -11 7 5 7.04 1.22 -11 7 5 9.43 1.64 -9 7 5 162.14 3.62 -9 7 5 212.89 5.09 -7 7 5 26.78 1.70 -7 7 5 34.36 2.36 -7 7 5 20.52 1.88 -5 7 5 38.53 2.36 -5 7 5 22.26 1.87 -5 7 5 38.47 2.98 -3 7 5 4.60 1.19 -3 7 5 2.29 0.92 -3 7 5 5.53 1.57 -1 7 5 96.47 3.25 -1 7 5 63.36 2.68 -1 7 5 94.28 4.00 1 7 5 327.61 5.63 1 7 5 218.63 4.65 1 7 5 315.81 6.81 3 7 5 295.13 5.30 3 7 5 214.49 4.54 3 7 5 276.34 6.35 5 7 5 138.06 3.68 5 7 5 104.36 3.22 5 7 5 122.75 4.35 7 7 5 101.14 3.19 7 7 5 88.35 3.74 7 7 5 85.02 3.54 9 7 5 0.07 0.69 9 7 5 0.28 1.01 9 7 5 0.59 0.98 11 7 5 11.41 1.52 11 7 5 11.42 1.92 13 7 5 326.56 5.47 13 7 5 333.53 6.88 15 7 5 7.08 1.26 15 7 5 8.40 1.69 17 7 5 43.00 2.26 17 7 5 46.56 2.88 19 7 5 71.32 2.78 21 7 5 35.23 2.13 23 7 5 19.32 1.72 25 7 5 17.04 1.68 27 7 5 98.15 3.10 29 7 5 1.07 0.76 31 7 5 21.31 1.67 33 7 5 52.80 2.15 35 7 5 2.12 0.74 -35 -7 -5 2.02 0.95 37 7 5 34.35 1.67 -39 7 4 11.81 1.33 39 -7 -4 13.09 1.63 -37 7 4 10.83 1.37 37 -7 -4 11.42 1.68 -35 7 4 79.10 2.96 35 -7 -4 81.72 3.37 -33 7 4 -0.10 0.82 33 -7 -4 0.29 1.14 -31 7 4 -0.14 0.84 31 -7 -4 0.77 1.24 -29 7 4 15.02 1.86 29 -7 -4 16.90 2.35 -27 7 4 24.50 2.14 27 -7 -4 25.43 2.77 -25 7 4 18.48 1.99 -25 7 4 10.73 1.88 25 -7 -4 14.93 2.27 -23 7 4 99.34 3.57 -23 7 4 77.64 3.65 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15.51 1.61 18 8 6 154.95 3.67 20 8 6 133.92 3.36 22 8 6 0.70 0.68 24 8 6 38.89 1.89 26 8 6 0.92 0.68 28 8 6 87.12 2.28 30 8 6 45.75 1.58 34 -8 -5 10.55 1.55 -32 8 5 7.63 0.92 32 -8 -5 8.61 1.57 -30 8 5 0.62 0.64 30 -8 -5 1.13 1.07 -28 8 5 92.23 2.57 28 -8 -5 102.10 3.83 -26 8 5 0.38 0.70 26 -8 -5 -0.31 1.14 -24 8 5 36.62 1.86 -24 8 5 30.21 2.54 24 -8 -5 35.32 2.80 -22 8 5 11.80 1.38 -22 8 5 9.89 1.80 22 -8 -5 9.12 1.90 -20 8 5 18.67 1.54 -20 8 5 18.97 2.23 20 -8 -5 18.93 2.41 -18 8 5 70.27 2.35 -18 8 5 77.50 3.51 -16 8 5 24.38 2.37 -14 8 5 -0.85 0.99 -12 8 5 41.15 2.68 -10 8 5 50.73 2.81 -8 8 5 0.75 0.94 -6 8 5 102.08 3.57 -4 8 5 28.84 2.20 -2 8 5 308.35 5.68 0 8 5 0.24 0.87 2 8 5 24.71 1.96 4 8 5 12.55 1.60 6 8 5 0.54 0.76 6 8 5 0.12 0.99 8 8 5 7.22 1.26 8 8 5 6.24 1.53 8 8 5 8.32 1.87 10 8 5 5.92 1.15 10 8 5 6.38 1.58 12 8 5 0.96 0.78 12 8 5 0.73 1.14 14 8 5 238.71 4.46 14 8 5 258.29 6.14 16 8 5 29.46 1.86 16 8 5 28.51 2.48 18 8 5 36.98 1.97 18 8 5 37.27 2.65 20 8 5 23.47 1.68 20 8 5 20.00 2.24 22 8 5 17.72 1.54 24 8 5 130.67 3.07 26 8 5 5.83 0.98 28 8 5 16.74 1.35 30 8 5 0.14 0.58 32 8 5 29.73 1.27 -34 8 4 10.50 1.10 34 -8 -4 10.47 1.56 -32 8 4 16.85 1.35 32 -8 -4 20.25 2.05 -30 8 4 14.98 1.40 30 -8 -4 16.65 2.12 -28 8 4 5.29 1.00 28 -8 -4 6.07 1.60 -26 8 4 69.89 2.48 -26 8 4 66.82 3.29 26 -8 -4 76.19 3.57 -24 8 4 48.67 2.16 -24 8 4 45.71 2.89 24 -8 -4 49.04 3.12 -22 8 4 2.78 0.89 -22 8 4 2.41 1.25 22 -8 -4 3.46 1.55 -20 8 4 111.20 2.94 -20 8 4 107.11 4.00 -18 8 4 65.53 2.26 -18 8 4 76.07 3.46 -16 8 4 1.11 1.09 -14 8 4 209.46 5.15 -12 8 4 168.11 4.58 -10 8 4 23.37 2.10 -10 8 4 18.97 2.60 -8 8 4 49.30 2.59 -8 8 4 39.63 2.73 -6 8 4 15.88 1.78 -6 8 4 11.08 1.84 -4 8 4 41.94 2.35 -4 8 4 34.49 2.59 -2 8 4 253.86 4.89 -2 8 4 202.48 5.37 0 8 4 61.28 2.56 0 8 4 45.38 2.89 2 8 4 32.53 2.02 2 8 4 29.36 2.44 4 8 4 22.37 1.72 4 8 4 19.45 2.15 6 8 4 101.10 2.95 6 8 4 87.58 3.77 8 8 4 67.07 2.46 8 8 4 59.65 3.24 10 8 4 259.21 4.39 10 8 4 243.10 6.04 10 8 4 189.76 3.54 10 8 4 284.89 6.68 12 8 4 7.13 1.15 12 8 4 6.61 1.63 12 8 4 5.51 0.89 12 8 4 9.75 1.90 14 8 4 45.25 2.04 14 8 4 30.99 1.58 14 8 4 46.79 3.10 16 8 4 0.78 0.71 16 8 4 0.18 0.48 16 8 4 1.33 1.20 18 8 4 55.24 2.17 18 8 4 33.81 1.69 18 8 4 55.09 3.22 20 8 4 50.32 2.08 20 8 4 55.22 3.17 22 8 4 140.74 3.12 22 8 4 136.96 4.56 24 8 4 54.30 2.06 26 8 4 3.26 0.84 28 8 4 0.67 0.64 30 8 4 22.55 1.34 32 8 4 78.76 1.86 -36 8 3 15.45 1.15 36 -8 -3 20.77 1.94 -34 8 3 1.53 0.69 34 -8 -3 2.32 1.16 -32 8 3 95.13 2.65 32 -8 -3 107.56 3.81 -30 8 3 14.34 1.44 30 -8 -3 14.70 2.02 -28 8 3 7.12 1.16 -28 8 3 7.46 1.65 28 -8 -3 7.39 1.67 -26 8 3 -0.33 0.68 -26 8 3 0.53 1.09 26 -8 -3 -0.03 1.27 -24 8 3 4.49 1.00 -24 8 3 3.98 1.38 -24 8 3 2.84 1.27 24 -8 -3 3.76 1.62 -22 8 3 20.75 1.61 -22 8 3 21.35 2.30 -22 8 3 17.21 2.14 -20 8 3 53.23 2.15 -20 8 3 49.58 2.92 -20 8 3 48.43 2.98 -18 8 3 27.50 1.73 -18 8 3 35.03 2.55 -18 8 3 30.59 2.52 -16 8 3 28.85 2.36 -16 8 3 23.77 2.33 -14 8 3 61.47 3.00 -14 8 3 50.53 3.01 -12 8 3 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9.55 1.50 -15 9 7 2.51 1.15 -13 9 7 17.70 1.96 -11 9 7 114.39 3.61 -9 9 7 73.00 3.00 -7 9 7 1.73 1.04 -5 9 7 0.55 0.93 -3 9 7 1.74 0.96 -1 9 7 10.22 1.49 1 9 7 96.70 3.16 1 9 7 90.50 3.56 3 9 7 125.89 3.49 3 9 7 118.87 3.97 5 9 7 0.83 0.87 5 9 7 0.95 1.05 7 9 7 0.88 0.85 9 9 7 19.96 1.61 11 9 7 102.60 2.82 13 9 7 12.73 1.38 15 9 7 24.74 1.54 17 9 7 9.69 1.15 19 9 7 0.31 0.56 -23 9 6 37.75 2.34 23 -9 -6 36.02 2.47 -21 9 6 25.47 2.16 -19 9 6 49.54 2.66 -17 9 6 4.70 1.29 -15 9 6 24.05 2.17 -13 9 6 34.30 2.40 -11 9 6 91.60 3.35 -9 9 6 30.76 2.25 -7 9 6 18.57 1.92 -5 9 6 31.73 2.19 -3 9 6 30.33 2.14 -1 9 6 38.51 2.28 1 9 6 2.03 1.01 3 9 6 137.25 3.61 5 9 6 32.24 2.04 5 9 6 33.25 2.63 7 9 6 24.69 1.83 7 9 6 22.91 2.31 9 9 6 73.50 2.58 9 9 6 66.59 3.23 11 9 6 84.15 2.63 11 9 6 77.66 3.35 13 9 6 0.72 0.75 13 9 6 0.60 1.10 15 9 6 31.12 1.69 17 9 6 19.62 1.38 19 9 6 10.09 1.13 21 9 6 68.91 1.79 27 -9 -5 20.98 2.02 -25 9 5 68.20 2.94 25 -9 -5 74.27 3.16 -23 9 5 72.49 3.05 -21 9 5 1.09 1.03 -19 9 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79.14 2.48 7 9 4 77.38 3.62 7 9 4 85.27 3.98 9 9 4 24.39 1.59 9 9 4 23.42 2.37 9 9 4 29.18 2.66 11 9 4 10.35 1.27 11 9 4 10.47 1.88 11 9 4 11.82 2.03 13 9 4 46.65 1.79 13 9 4 54.60 3.24 15 9 4 19.74 2.54 17 9 4 68.97 3.40 19 9 4 61.81 2.31 19 9 4 91.89 3.77 21 9 4 5.89 1.53 31 -9 -3 9.01 1.48 -29 9 3 2.24 1.04 29 -9 -3 0.89 1.12 -27 9 3 2.81 1.15 27 -9 -3 3.15 1.31 -25 9 3 -0.04 1.01 -23 9 3 53.00 2.84 -21 9 3 44.19 2.67 -21 9 3 32.45 2.45 -19 9 3 141.81 4.23 -19 9 3 113.34 4.06 -17 9 3 1.37 1.07 -17 9 3 2.30 1.27 -15 9 3 14.84 1.85 -15 9 3 17.41 2.21 -13 9 3 7.79 1.45 -13 9 3 9.83 1.77 -11 9 3 65.86 2.89 -11 9 3 63.26 3.34 -9 9 3 1.53 1.02 -9 9 3 1.07 1.14 -7 9 3 12.23 1.58 -7 9 3 11.59 1.94 -5 9 3 26.97 1.92 -5 9 3 22.52 2.39 -3 9 3 2.43 0.96 -3 9 3 2.16 1.23 -1 9 3 1.00 0.81 -1 9 3 -0.07 1.03 1 9 3 192.63 3.74 1 9 3 179.05 5.34 3 9 3 25.00 1.61 3 9 3 24.79 2.44 5 9 3 2.45 0.82 5 9 3 2.19 1.20 7 9 3 164.84 3.02 7 9 3 168.00 5.21 7 9 3 186.68 5.68 9 9 3 23.71 2.47 9 9 3 26.83 2.69 11 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1.11 5 9 2 1.55 1.32 7 9 2 0.56 0.63 7 9 2 1.68 1.25 7 9 2 1.11 1.24 9 9 2 5.41 0.89 9 9 2 7.93 1.79 9 9 2 8.03 1.88 11 9 2 136.75 2.57 11 9 2 187.17 5.64 11 9 2 139.34 2.37 11 9 2 191.51 5.73 13 9 2 16.14 1.17 13 9 2 24.31 2.57 13 9 2 16.83 0.96 13 9 2 24.74 2.62 15 9 2 49.70 1.68 15 9 2 70.83 3.70 15 9 2 50.17 1.49 15 9 2 71.73 3.79 17 9 2 0.55 0.60 17 9 2 1.05 0.41 17 9 2 1.03 1.25 19 9 2 0.50 0.55 19 9 2 0.37 0.39 19 9 2 1.01 1.27 21 9 2 31.44 1.45 21 9 2 26.40 1.22 21 9 2 48.83 3.13 23 9 2 71.23 1.99 23 9 2 58.64 1.75 25 9 2 18.62 1.26 25 9 2 17.94 1.09 27 9 2 2.12 0.56 29 9 2 1.00 0.48 31 9 2 1.92 0.66 33 9 2 46.99 1.49 -33 9 1 9.73 1.42 -31 9 1 5.01 1.27 -31 9 1 4.48 1.21 31 -9 -1 4.32 1.27 -29 9 1 29.54 2.28 -29 9 1 28.84 2.25 29 -9 -1 30.59 2.42 -27 9 1 47.10 2.68 -27 9 1 36.58 2.55 -25 9 1 56.25 2.86 -25 9 1 42.69 2.80 -23 9 1 14.45 1.90 -23 9 1 10.83 1.86 -21 9 1 0.61 1.03 -21 9 1 0.65 1.17 -19 9 1 192.42 4.81 -19 9 1 157.75 5.03 -17 9 1 5.11 1.36 -17 9 1 4.82 1.49 -15 9 1 24.66 2.13 -15 9 1 23.62 2.45 -13 9 1 51.02 2.59 -13 9 1 53.07 3.24 -11 9 1 0.83 0.87 -11 9 1 0.89 1.17 -9 9 1 16.19 1.70 -9 9 1 19.01 2.49 -7 9 1 231.81 4.41 -7 9 1 201.49 4.09 -7 9 1 278.47 6.72 -5 9 1 72.06 2.52 -5 9 1 61.49 2.31 -5 9 1 100.67 4.27 -3 9 1 10.87 1.29 -3 9 1 8.44 1.12 -3 9 1 16.18 2.40 -1 9 1 12.95 1.31 -1 9 1 16.97 2.34 1 9 1 55.27 1.85 1 9 1 79.06 3.87 3 9 1 23.17 1.39 3 9 1 27.12 2.67 5 9 1 33.30 1.42 5 9 1 37.37 2.98 5 9 1 36.93 2.97 7 9 1 33.29 1.33 7 9 1 42.88 3.04 7 9 1 42.74 3.14 9 9 1 4.03 1.47 9 9 1 4.53 1.63 11 9 1 0.71 1.18 11 9 1 0.79 1.19 13 9 1 31.96 2.76 13 9 1 32.83 2.88 15 9 1 102.75 4.35 15 9 1 107.64 4.46 17 9 1 9.33 1.85 17 9 1 11.57 2.25 19 9 1 1.02 0.51 19 9 1 1.84 1.43 21 9 1 30.21 1.25 21 9 1 23.20 1.03 21 9 1 44.27 3.06 23 9 1 4.56 0.72 23 9 1 3.84 0.58 25 9 1 3.96 0.71 25 9 1 2.95 0.55 27 9 1 30.32 1.34 27 9 1 27.57 1.22 29 9 1 7.11 0.87 29 9 1 3.90 0.71 29 9 1 3.99 0.63 31 9 1 25.73 1.26 31 9 1 19.40 1.15 33 9 1 50.13 1.46 33 9 1 35.61 1.33 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2.15 -18 10 1 28.68 2.46 -16 10 1 98.73 3.18 -16 10 1 81.81 3.63 -14 10 1 9.44 1.39 -14 10 1 8.27 1.69 -12 10 1 13.76 1.64 -12 10 1 13.69 2.06 -10 10 1 49.40 2.26 -10 10 1 50.78 3.17 -8 10 1 72.64 2.53 -8 10 1 73.79 3.66 -6 10 1 9.24 1.27 -6 10 1 9.82 1.85 -4 10 1 47.11 1.91 -4 10 1 50.23 3.22 -2 10 1 5.00 1.57 -2 10 1 8.53 1.84 0 10 1 6.02 1.60 0 10 1 6.60 1.67 2 10 1 36.53 2.85 2 10 1 38.70 3.00 4 10 1 27.24 1.42 4 10 1 28.97 2.61 4 10 1 31.04 2.80 6 10 1 59.33 1.75 6 10 1 66.17 3.56 6 10 1 74.42 3.77 8 10 1 154.76 5.08 8 10 1 166.00 5.27 10 10 1 9.27 1.93 10 10 1 9.09 1.91 12 10 1 84.82 3.90 12 10 1 86.37 3.93 14 10 1 12.07 1.99 14 10 1 10.45 2.01 16 10 1 11.22 2.06 18 10 1 160.88 4.91 -28 10 0 2.88 1.03 -26 10 0 36.19 2.04 -26 10 0 32.76 2.20 -24 10 0 34.64 2.08 -24 10 0 25.04 2.15 -22 10 0 31.44 2.08 -22 10 0 23.71 2.20 -20 10 0 6.33 1.27 -20 10 0 4.22 1.38 -18 10 0 6.16 1.26 -18 10 0 5.45 1.49 -16 10 0 27.77 1.99 -16 10 0 23.19 2.36 -14 10 0 1.88 0.94 -14 10 0 2.27 1.30 -12 10 0 2.31 0.94 -12 10 0 1.41 1.24 -10 10 0 6.05 1.15 -10 10 0 4.20 1.47 -8 10 0 20.64 1.64 -8 10 0 17.80 2.32 -6 10 0 28.85 1.69 -6 10 0 31.72 2.75 -6 10 0 30.02 2.63 -4 10 0 88.69 2.29 -4 10 0 81.68 3.91 -4 10 0 83.75 3.81 -2 10 0 0.09 1.13 -2 10 0 0.60 1.13 0 10 0 4.98 1.57 0 10 0 5.69 1.62 2 10 0 1.10 1.16 2 10 0 1.77 1.25 4 10 0 85.15 3.96 4 10 0 88.30 3.99 6 10 0 33.76 2.79 6 10 0 32.83 2.76 8 10 0 21.52 2.48 8 10 0 23.12 2.55 10 10 0 5.79 1.63 10 10 0 5.60 1.65 12 10 0 2.11 1.29 12 10 0 2.18 1.28 14 10 0 1.81 1.34 14 10 0 1.06 1.26 16 10 0 26.52 2.55 18 10 0 6.56 1.64 -28 10 -1 2.07 0.98 -26 10 -1 1.32 0.80 -26 10 -1 0.60 0.92 -24 10 -1 3.07 1.01 -24 10 -1 3.10 1.21 -22 10 -1 7.63 1.30 -22 10 -1 6.40 1.45 -20 10 -1 33.48 2.07 -20 10 -1 25.65 2.31 -18 10 -1 174.05 4.02 -18 10 -1 140.41 4.55 -16 10 -1 9.08 1.38 -16 10 -1 7.89 1.72 -14 10 -1 8.67 1.33 -14 10 -1 9.07 1.76 -12 10 -1 80.47 2.74 -12 10 -1 76.65 3.71 -10 10 -1 9.53 1.26 -10 10 -1 8.96 1.81 -8 10 -1 155.10 3.31 -8 10 -1 111.49 3.09 -8 10 -1 139.72 4.84 -8 10 -1 129.25 4.54 -6 10 -1 69.16 2.21 -6 10 -1 47.53 2.11 -6 10 -1 60.35 3.43 -6 10 -1 58.32 3.24 -4 10 -1 33.88 1.55 -4 10 -1 22.97 1.57 -4 10 -1 32.35 2.80 -4 10 -1 25.91 2.51 -2 10 -1 23.04 1.48 -2 10 -1 34.73 2.90 -2 10 -1 34.37 2.71 0 10 -1 3.72 0.81 0 10 -1 7.78 1.79 0 10 -1 6.16 1.73 2 10 -1 5.28 0.82 2 10 -1 5.99 1.72 2 10 -1 8.62 1.79 4 10 -1 40.90 1.42 4 10 -1 51.42 3.27 4 10 -1 51.33 3.18 6 10 -1 9.55 1.82 6 10 -1 9.27 1.88 8 10 -1 75.94 3.77 8 10 -1 76.63 3.70 10 10 -1 51.64 3.22 10 10 -1 51.85 3.19 12 10 -1 15.40 2.24 12 10 -1 14.97 2.31 14 10 -1 9.75 1.91 14 10 -1 9.38 1.88 16 10 -1 91.28 3.87 16 10 -1 86.02 3.78 -28 10 -2 35.32 2.11 -26 10 -2 -0.55 0.68 -26 10 -2 0.33 0.88 -24 10 -2 18.93 1.66 -24 10 -2 16.50 1.87 -22 10 -2 4.97 1.10 -22 10 -2 4.41 1.33 -20 10 -2 -0.11 0.76 -20 10 -2 1.38 1.11 -18 10 -2 64.73 2.60 -18 10 -2 59.59 3.12 -16 10 -2 53.41 2.38 -16 10 -2 50.26 3.02 -14 10 -2 8.79 1.27 -14 10 -2 8.29 1.70 -12 10 -2 107.96 3.04 -12 10 -2 100.78 4.10 -10 10 -2 0.60 0.77 -10 10 -2 -0.59 1.08 -8 10 -2 0.28 0.70 -8 10 -2 0.02 0.75 -8 10 -2 0.30 1.07 -6 10 -2 53.28 1.97 -6 10 -2 41.93 2.01 -6 10 -2 49.20 3.16 -4 10 -2 149.45 2.71 -4 10 -2 120.21 2.93 -4 10 -2 141.60 4.86 -2 10 -2 5.52 0.96 -2 10 -2 7.63 1.76 0 10 -2 24.33 1.44 0 10 -2 26.56 2.60 0 10 -2 25.34 2.44 2 10 -2 0.49 0.57 2 10 -2 -1.07 1.10 2 10 -2 -0.58 1.15 4 10 -2 6.32 0.81 4 10 -2 6.32 1.65 4 10 -2 6.60 1.65 6 10 -2 56.19 3.27 6 10 -2 54.36 3.14 8 10 -2 143.00 4.80 8 10 -2 138.99 4.61 10 10 -2 27.16 2.54 10 10 -2 27.96 2.56 12 10 -2 7.48 1.73 12 10 -2 6.33 1.61 14 10 -2 12.76 2.05 -26 10 -3 92.12 3.09 -24 10 -3 -0.39 0.64 -24 10 -3 0.73 0.91 -22 10 -3 27.92 1.82 -22 10 -3 22.36 2.04 -20 10 -3 0.44 0.73 -20 10 -3 0.02 0.97 -18 10 -3 1.54 0.84 -18 10 -3 0.68 1.05 -16 10 -3 56.58 2.39 -16 10 -3 54.36 3.02 -14 10 -3 67.94 2.52 -14 10 -3 64.96 3.26 -12 10 -3 4.37 0.99 -12 10 -3 3.96 1.40 -10 10 -3 41.14 1.96 -10 10 -3 38.28 2.75 -8 10 -3 12.57 1.35 -8 10 -3 9.05 1.32 -8 10 -3 12.59 2.03 -6 10 -3 -0.11 0.62 -6 10 -3 0.66 0.76 -6 10 -3 -0.15 1.01 -4 10 -3 97.56 2.26 -4 10 -3 82.11 2.55 -4 10 -3 99.23 4.04 -2 10 -3 15.46 1.37 -2 10 -3 17.15 2.24 0 10 -3 11.77 1.23 0 10 -3 10.76 1.89 2 10 -3 4.00 0.81 2 10 -3 4.37 1.44 4 10 -3 1.62 0.61 4 10 -3 1.78 1.20 6 10 -3 39.46 1.40 6 10 -3 41.89 2.83 8 10 -3 91.25 3.84 8 10 -3 75.78 3.44 10 10 -3 -0.53 1.06 12 10 -3 1.01 1.16 14 10 -3 1.50 1.22 -24 10 -4 1.02 1.06 -22 10 -4 0.87 0.72 -22 10 -4 1.33 0.96 -20 10 -4 9.01 1.26 -20 10 -4 8.72 1.47 -18 10 -4 21.66 1.66 -18 10 -4 20.34 2.04 -16 10 -4 76.76 2.60 -16 10 -4 72.90 3.18 -14 10 -4 29.04 1.78 -14 10 -4 26.92 2.27 -12 10 -4 19.99 1.59 -12 10 -4 20.03 2.15 -10 10 -4 3.79 0.93 -10 10 -4 4.15 1.36 -8 10 -4 0.30 0.68 -8 10 -4 -0.37 1.00 -6 10 -4 49.06 1.86 -6 10 -4 43.33 2.11 -6 10 -4 47.01 2.87 -4 10 -4 63.91 1.93 -4 10 -4 61.30 2.29 -4 10 -4 58.27 3.15 -2 10 -4 28.73 1.68 -2 10 -4 31.47 2.59 0 10 -4 60.06 2.08 0 10 -4 63.54 3.25 2 10 -4 20.29 1.38 2 10 -4 18.73 2.25 4 10 -4 8.09 1.00 4 10 -4 9.86 1.75 6 10 -4 12.08 1.11 6 10 -4 12.68 1.91 8 10 -4 11.44 1.02 8 10 -4 9.57 1.69 10 10 -4 16.83 2.08 12 10 -4 17.28 2.06 -20 10 -5 10.34 1.26 -18 10 -5 38.06 1.86 -18 10 -5 34.04 2.15 -16 10 -5 41.85 1.92 -16 10 -5 38.65 2.32 -14 10 -5 4.11 0.92 -14 10 -5 3.51 1.22 -12 10 -5 85.16 2.51 -12 10 -5 76.85 3.14 -10 10 -5 0.92 0.67 -10 10 -5 1.12 1.09 -8 10 -5 90.14 2.46 -8 10 -5 82.48 3.35 -6 10 -5 18.38 1.33 -6 10 -5 17.18 1.98 -4 10 -5 40.91 1.63 -4 10 -5 36.42 1.91 -4 10 -5 36.71 2.58 0 10 -5 134.01 3.02 2 10 -5 24.23 1.51 4 10 -5 23.50 1.45 6 10 -5 10.17 1.13 8 10 -5 53.29 1.73 10 10 -5 51.12 1.61 12 10 -5 21.35 1.12 14 10 -5 51.31 1.37 16 10 -5 5.60 0.67 -16 10 -6 2.60 0.76 -14 10 -6 56.41 1.99 -12 10 -6 16.02 1.32 -10 10 -6 12.85 1.24 -8 10 -6 2.56 0.78 -6 10 -6 1.13 0.60 -4 10 -6 70.72 1.90 -2 10 -6 14.56 1.47 0 10 -6 18.74 1.52 2 10 -6 0.97 0.70 4 10 -6 10.18 1.16 6 10 -6 6.99 0.96 8 10 -6 45.37 1.68 10 10 -6 16.28 1.19 12 10 -6 15.93 1.11 14 10 -6 45.66 1.38 16 10 -6 15.90 0.91 16 10 -6 14.13 0.87 -10 10 -7 11.88 1.11 -8 10 -7 25.09 1.29 -6 10 -7 2.54 0.62 -4 10 -7 21.21 1.11 0 10 -7 88.13 2.48 2 10 -7 1.03 0.74 4 10 -7 9.53 1.13 6 10 -7 8.68 1.03 8 10 -7 28.24 1.42 10 10 -7 2.17 0.64 12 10 -7 16.29 1.09 14 10 -7 11.02 0.92 -7 11 5 53.80 1.64 -13 11 4 0.76 0.66 -11 11 4 20.38 1.37 -9 11 4 4.13 0.81 -9 11 4 5.04 1.35 -7 11 4 4.83 0.79 -7 11 4 5.45 1.41 -5 11 4 12.11 1.79 -3 11 4 0.38 1.03 -1 11 4 -0.01 0.98 1 11 4 45.48 2.43 1 11 4 55.82 2.88 3 11 4 48.97 2.70 5 11 4 6.72 1.42 7 11 4 4.37 1.25 9 11 4 18.60 1.19 9 11 4 26.63 2.12 11 11 4 7.74 0.84 13 11 4 47.00 1.32 -17 11 3 8.53 1.06 -15 11 3 84.60 2.30 -13 11 3 25.29 1.48 -13 11 3 15.94 1.76 -11 11 3 0.06 0.63 -11 11 3 0.47 0.93 -9 11 3 0.95 0.68 -9 11 3 0.83 0.97 -9 11 3 1.53 1.15 -7 11 3 7.08 0.87 -7 11 3 9.35 1.52 -7 11 3 8.09 1.66 -5 11 3 9.41 1.59 -5 11 3 13.25 1.95 -3 11 3 137.56 4.09 -3 11 3 159.89 4.61 -1 11 3 19.74 2.03 -1 11 3 21.44 2.21 1 11 3 0.62 0.97 1 11 3 0.30 1.08 3 11 3 1.22 1.08 3 11 3 1.49 1.15 5 11 3 13.35 1.83 5 11 3 14.24 1.92 7 11 3 48.61 2.77 9 11 3 134.20 4.11 11 11 3 28.52 2.21 13 11 3 2.20 1.10 -19 11 2 0.72 0.68 -17 11 2 2.88 0.85 -17 11 2 1.24 1.04 -15 11 2 44.74 1.84 -15 11 2 34.56 2.30 -13 11 2 55.25 1.94 -13 11 2 46.15 2.56 -11 11 2 -0.29 0.61 -11 11 2 -0.47 0.91 -11 11 2 0.55 1.06 -9 11 2 5.48 0.88 -9 11 2 6.31 1.45 -9 11 2 7.20 1.55 -7 11 2 3.54 1.26 -7 11 2 3.76 1.35 -5 11 2 2.58 1.19 -5 11 2 2.38 1.27 -3 11 2 10.83 1.76 -3 11 2 11.58 1.88 -1 11 2 7.94 1.63 -1 11 2 7.29 1.68 1 11 2 -0.31 1.04 1 11 2 0.21 1.05 3 11 2 9.38 1.68 3 11 2 9.45 1.78 5 11 2 8.05 1.64 5 11 2 6.60 1.60 7 11 2 18.53 2.12 7 11 2 20.96 2.21 9 11 2 6.90 1.52 9 11 2 6.89 1.57 11 11 2 1.20 1.08 13 11 2 27.61 2.25 15 11 2 18.84 1.99 -19 11 1 5.01 0.87 -19 11 1 2.29 1.07 -17 11 1 27.43 1.55 -17 11 1 20.16 1.95 -15 11 1 4.50 0.88 -15 11 1 4.11 1.26 -13 11 1 23.83 1.46 -13 11 1 24.01 2.15 -13 11 1 22.67 2.07 -11 11 1 57.68 1.86 -11 11 1 55.15 2.89 -11 11 1 55.37 2.84 -9 11 1 42.89 1.55 -9 11 1 45.34 2.78 -9 11 1 41.73 2.62 -7 11 1 50.96 2.90 -7 11 1 48.54 2.83 -5 11 1 8.28 1.66 -5 11 1 8.14 1.66 -3 11 1 6.18 1.52 -3 11 1 5.35 1.50 -1 11 1 23.22 2.25 -1 11 1 21.26 2.25 1 11 1 97.57 3.82 1 11 1 100.58 3.87 3 11 1 30.31 2.47 3 11 1 30.33 2.50 5 11 1 8.97 1.65 5 11 1 9.20 1.74 7 11 1 112.99 4.02 7 11 1 113.26 4.04 9 11 1 59.40 3.07 9 11 1 62.17 3.14 11 11 1 103.72 3.78 11 11 1 113.14 3.96 13 11 1 140.75 4.26 15 11 1 42.47 2.58 -21 11 0 18.32 1.77 -19 11 0 45.54 1.78 -19 11 0 37.58 2.27 -17 11 0 3.01 0.79 -17 11 0 2.76 1.11 -15 11 0 2.12 0.74 -15 11 0 1.41 1.04 -13 11 0 11.54 1.17 -13 11 0 12.74 1.84 -11 11 0 2.18 0.71 -11 11 0 2.52 1.25 -9 11 0 1.10 1.07 -9 11 0 1.22 1.17 -7 11 0 3.18 1.27 -7 11 0 4.60 1.39 -5 11 0 23.76 2.31 -5 11 0 24.49 2.26 -3 11 0 7.94 1.70 -3 11 0 5.67 1.49 -1 11 0 50.72 2.98 -1 11 0 52.11 2.95 1 11 0 54.34 3.05 1 11 0 49.95 2.90 3 11 0 6.99 1.56 3 11 0 5.08 1.46 5 11 0 25.76 2.37 5 11 0 23.39 2.29 7 11 0 4.38 1.44 7 11 0 5.74 1.49 9 11 0 1.62 1.20 9 11 0 1.66 1.19 11 11 0 1.52 1.19 11 11 0 2.30 1.24 13 11 0 14.36 2.01 -21 11 -1 -0.07 0.83 -19 11 -1 12.70 1.21 -19 11 -1 11.29 1.53 -17 11 -1 11.53 1.17 -17 11 -1 12.44 1.71 -15 11 -1 43.08 1.71 -15 11 -1 38.16 2.44 -13 11 -1 135.95 2.60 -13 11 -1 131.78 4.09 -11 11 -1 101.25 2.14 -11 11 -1 97.61 3.68 -9 11 -1 60.28 3.08 -7 11 -1 110.12 3.97 -5 11 -1 8.65 1.76 -3 11 -1 27.65 2.43 -3 11 -1 23.49 2.25 -1 11 -1 97.87 3.86 -1 11 -1 88.11 3.51 1 11 -1 20.44 2.20 1 11 -1 18.11 2.13 3 11 -1 6.65 1.53 3 11 -1 8.09 1.63 5 11 -1 12.88 1.95 5 11 -1 8.43 1.67 7 11 -1 51.65 2.94 7 11 -1 49.53 2.82 9 11 -1 49.38 2.85 9 11 -1 43.21 2.69 11 11 -1 60.07 3.05 11 11 -1 51.69 2.81 -19 11 -2 0.11 0.58 -19 11 -2 0.68 0.88 -17 11 -2 1.41 0.63 -17 11 -2 1.29 0.99 -15 11 -2 17.26 1.22 -15 11 -2 16.64 1.88 -13 11 -2 27.02 1.32 -13 11 -2 25.69 2.16 -11 11 -2 0.41 0.51 -11 11 -2 -0.08 1.03 -9 11 -2 5.39 1.44 -7 11 -2 17.83 2.07 -5 11 -2 5.60 0.93 -5 11 -2 6.32 1.54 -3 11 -2 6.12 0.90 -3 11 -2 7.46 1.58 -1 11 -2 0.18 1.05 1 11 -2 8.47 1.62 3 11 -2 8.51 1.65 5 11 -2 1.95 1.19 5 11 -2 2.55 1.34 7 11 -2 3.74 1.30 7 11 -2 4.00 1.35 9 11 -2 6.43 1.50 11 11 -2 0.20 0.98 -17 11 -3 1.35 0.94 -15 11 -3 17.12 1.11 -15 11 -3 16.54 1.79 -13 11 -3 2.29 0.60 -13 11 -3 1.20 1.12 -11 11 -3 23.25 2.07 -9 11 -3 95.68 2.54 -9 11 -3 117.67 3.78 -7 11 -3 34.17 1.66 -7 11 -3 39.49 2.55 -5 11 -3 11.13 1.19 -5 11 -3 11.88 1.80 -3 11 -3 0.84 0.61 -3 11 -3 -0.08 1.01 -1 11 -3 1.03 0.60 -1 11 -3 2.01 1.11 1 11 -3 21.83 1.14 1 11 -3 29.23 2.28 3 11 -3 144.17 4.21 5 11 -3 9.91 1.64 7 11 -3 9.32 1.62 9 11 -3 0.44 1.03 -11 11 -4 7.39 1.34 -9 11 -4 20.29 1.42 -9 11 -4 19.54 1.92 -7 11 -4 2.75 0.80 -7 11 -4 3.52 1.14 -5 11 -4 5.64 0.91 -5 11 -4 5.19 1.33 -3 11 -4 33.27 1.49 -3 11 -4 37.62 2.30 -1 11 -4 37.97 1.49 -1 11 -4 43.86 2.45 1 11 -4 0.72 0.54 1 11 -4 1.05 1.04 3 11 -4 0.40 0.47 3 11 -4 0.54 1.06 5 11 -4 9.45 1.53 7 11 -4 5.06 1.31 -5 11 -5 46.68 1.71 -3 11 -5 1.21 0.60 -1 11 -5 30.40 1.35 1 11 -5 42.80 1.43 3 11 -5 10.78 0.88 -2 12 1 16.43 1.75 0 12 1 1.23 0.96 2 12 1 2.62 1.06 4 12 1 1.20 0.96 -6 12 0 5.75 1.25 -4 12 0 16.27 1.69 -2 12 0 30.93 2.06 0 12 0 14.21 1.69 2 12 0 30.98 2.08 4 12 0 16.20 1.76 6 12 0 4.54 1.18 -4 12 -1 0.53 0.88 -2 12 -1 1.15 0.98 0 12 -1 3.03 1.09 2 12 -1 17.84 1.76 4 12 -1 10.42 1.49 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 63360 _olex2_submission_special_instructions 'No special instructions were received' _vrf_PLAT029_he015 ; PROBLEM: _diffrn_measured_fraction_theta_full value Low . 0.971 Why? RESPONSE: This is due to weak high angle data. ; _vrf_PLAT220_he015 ; PROBLEM: NonSolvent Resd 1 C Ueq(max) / Ueq(min) Range 4.5 Ratio RESPONSE: This is due to disordered in the di(pentan-3-yl) moiety. ; _vrf_PLAT222_he015 ; PROBLEM: NonSolvent Resd 1 H Uiso(max)/Uiso(min) Range 4.7 Ratio RESPONSE: This is due to disordered in the di(pentan-3-yl) moiety. ; _vrf_PLAT911_he015 ; PROBLEM: Missing FCF Refl Between Thmin & STh/L= 0.597 116 Report RESPONSE: The structure was collected to 97% completeness resulting in the missing reflections. ;